C₂₆H₃₈O₄Si₂

Base Information Edit

Chemical Name:C₂₆H₃₈O₄Si₂
CAS No.:929117-82-8
Molecular Formula:C₂₆H₃₈O₄Si₂
Molecular Weight:470.756
Hs Code.:
Mol file:929117-82-8.mol

C<sub>26</sub>H<sub>38</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₂₆H₃₈O₄Si₂

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Chemical Property of C₂₆H₃₈O₄Si₂ Edit

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Technology Process of C₂₆H₃₈O₄Si₂

There total 4 articles about C₂₆H₃₈O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 851278-46-1
(1R,2R,3R)-5-(tert-butyldiphenylsilyloxy)-1,2-epoxy-1-trimethylsilylpentan-3-ol

: 64-19-7,77671-22-8
acetic acid

: 929117-82-8
C₂₆H₃₈O₄Si₂

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; at 0 ℃; for 2h;
DOI:10.1021/jo0623890

Reference yield:

: 851278-45-0
(1E)-5-[(tert-butyldiphenylsilyl)oxy]-1-trimethylsilyl-1-penten-3-ol

: 929117-82-8
C₂₆H₃₈O₄Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: 47 percent / t-BuOOH; D-(-)-DIPT; Ti(O-i-Pr)4 / CH₂Cl₂ / 13 h / -20 °C

2: 80 percent / Ph₃P; DIAD / 2 h / 0 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; di-isopropyl azodicarboxylate; D-(-)-diisopropyl tartrate; triphenylphosphine; In dichloromethane; 1: Sharpless epoxidation / 2: Mitsunobu reaction;
DOI:10.1021/jo0623890

Reference yield:

: 58207-97-9
tributyl[(E)-2-trimethylsilylethenyl]stannane

: 929117-82-8
C₂₆H₃₈O₄Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 1.5 h / -70 - -60 °C

1.2: 91 percent / tetrahydrofuran; hexane / 3 h / -70 °C

2.1: 47 percent / t-BuOOH; D-(-)-DIPT; Ti(O-i-Pr)4 / CH₂Cl₂ / 13 h / -20 °C

3.1: 80 percent / Ph₃P; DIAD / 2 h / 0 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; n-butyllithium; di-isopropyl azodicarboxylate; D-(-)-diisopropyl tartrate; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane; 2.1: Sharpless epoxidation / 3.1: Mitsunobu reaction;
DOI:10.1021/jo0623890