(R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoyl chloride

Base Information

Chemical Name:(R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoyl chloride
CAS No.:1313429-37-6
Molecular Formula:C₁₃H₁₇ClO₂
Molecular Weight:240.73
Hs Code.:

Synonyms:(R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoyl chloride

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Chemical Property of (R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoyl chloride

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Technology Process of (R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoyl chloride

There total 30 articles about (R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1313429-32-1
(αR,βR)-β-ethyl-3-methoxy-α-methylbenzenepropanoic acid

: 1313429-37-6
(R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoyl chloride

Guidance literature:: With thionyl chloride; In toluene; at 75 - 80 ℃; for 3h;

Reference yield:

: 591-31-1
3-methoxy-benzaldehyde

: 1313429-37-6
(R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoyl chloride

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 6 h / 50 - 60 °C

2.1: tetrahydrofuran / -15 - 25 °C / Inert atmosphere

2.2: 0 - 5 °C

3.1: sodium hydride / toluene / 1 h / 20 °C / Inert atmosphere

3.2: 4 h / 45 - 50 °C

3.3: 0 - 5 °C / pH 1

4.1: lithium chloride / dimethyl sulfoxide / 15 h / 150 - 160 °C

5.1: sodium hydroxide / ethylene glycol / 4 h / 170 - 180 °C

5.2: pH 1

6.1: di-isopropyl ether / 6 h / 20 - 75 °C

7.1: hydrogenchloride / water; tert-butyl methyl ether / 0.5 h / 20 - 25 °C

8.1: thionyl chloride / toluene / 3 h / 75 - 80 °C

With hydrogenchloride; thionyl chloride; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; sodium hydroxide; In tetrahydrofuran; tert-butyl methyl ether; di-isopropyl ether; water; ethylene glycol; dimethyl sulfoxide; toluene;

Reference yield:

: 2972-72-7
2-(3-methoxybenzylidene)malononitrile

: 1313429-37-6
(R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoyl chloride

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetrahydrofuran / -15 - 25 °C / Inert atmosphere

1.2: 0 - 5 °C

2.1: potassium carbonate / dimethyl sulfoxide / 0.25 h / 25 °C

2.2: 1 h / 25 °C

3.1: tri-n-butyl-tin hydride / 2,2'-azobis(isobutyronitrile) / toluene / 10 h / Reflux

3.2: 20 °C

4.1: sodium hydroxide / ethylene glycol / 4 h / 170 - 180 °C

4.2: pH 1

5.1: di-isopropyl ether / 6 h / 20 - 75 °C

6.1: hydrogenchloride / water; tert-butyl methyl ether / 0.5 h / 20 - 25 °C

7.1: thionyl chloride / toluene / 3 h / 75 - 80 °C

With hydrogenchloride; thionyl chloride; tri-n-butyl-tin hydride; potassium carbonate; sodium hydroxide; 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; tert-butyl methyl ether; di-isopropyl ether; water; ethylene glycol; dimethyl sulfoxide; toluene;