H-D-Phe-Pro-Gly-ProψGly-OH

Base Information

Chemical Name:H-D-Phe-Pro-Gly-ProψGly-OH
CAS No.:99726-41-7
Molecular Formula:C₂₃H₃₂N₄O₅S
Molecular Weight:476.597
Hs Code.:

Synonyms:H-D-Phe-Pro-Gly-ProψGly-OH

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Chemical Property of H-D-Phe-Pro-Gly-ProψGly-OH

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Technology Process of H-D-Phe-Pro-Gly-ProψGly-OH

There total 4 articles about H-D-Phe-Pro-Gly-ProψGly-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69610-40-8
N-(tert-butoxycarbonyl)-L-prolinol

: 99726-41-7
H-D-Phe-Pro-Gly-ProψGly-OH

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / DMAP / dimethylformamide / 1.) 0 deg C, 0.5 h, 2.) room temp., 6 h

2: 38 percent / dimethylformamide; aq. KOH / 30 h

3: cesium carbonate / H₂O; methanol / 0.25 h

4: by a solid-phase synthesis

With caesium carbonate; dmap; In methanol; potassium hydroxide; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00264a041

Reference yield:

: 23356-96-9
(S)-1-Pyrrolidin-2-yl-methanol

: 99726-41-7
H-D-Phe-Pro-Gly-ProψGly-OH

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / ethyl acetate / 2 h / Ambient temperature

2: 83 percent / DMAP / dimethylformamide / 1.) 0 deg C, 0.5 h, 2.) room temp., 6 h

3: 38 percent / dimethylformamide; aq. KOH / 30 h

4: cesium carbonate / H₂O; methanol / 0.25 h

5: by a solid-phase synthesis

With caesium carbonate; dmap; In methanol; potassium hydroxide; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ja00264a041

Reference yield:

: 86661-32-7
(S)-tert-butyl 2-((tosyloxy)methyl)pyrrolidine-1-carboxylate

: 99726-41-7
H-D-Phe-Pro-Gly-ProψGly-OH

Guidance literature:: Multi-step reaction with 3 steps

1: 38 percent / dimethylformamide; aq. KOH / 30 h

2: cesium carbonate / H₂O; methanol / 0.25 h

3: by a solid-phase synthesis

With caesium carbonate; In methanol; potassium hydroxide; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00264a041