2-methyl-N,N-dimethyl-3-phenylpropanamide

Base Information

Chemical Name:2-methyl-N,N-dimethyl-3-phenylpropanamide
CAS No.:20929-40-2
Molecular Formula:C₁₂H₁₇NO
Molecular Weight:191.273
Hs Code.:

Synonyms:2-methyl-N,N-dimethyl-3-phenylpropanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methyl-N,N-dimethyl-3-phenylpropanamide

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Technology Process of 2-methyl-N,N-dimethyl-3-phenylpropanamide

There total 8 articles about 2-methyl-N,N-dimethyl-3-phenylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 512-56-1
trimethyl phosphite

: 5830-31-9
N,N-dimethyl-3-phenylpropanamide

: 20929-40-2
2-methyl-N,N-dimethyl-3-phenylpropanamide

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at 0 - 75 ℃; for 24h;
DOI:10.1055/a-1504-8366

Reference yield: 99.0%

: 20929-40-2
2-methyl-N,N-dimethyl-3-phenylpropanamide

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at 0 ℃; for 0.25h;

In tetrahydrofuran; at 80 ℃; for 24h;

Reference yield: 77.0%

: 300-57-2,57807-91-7
allylbenzene

: 201230-82-2
carbon monoxide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 35256-93-0
N,N-dimethyl-4-phenylbutanamide

: 20929-40-2
2-methyl-N,N-dimethyl-3-phenylpropanamide

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); N-methyl-2-pyrrolidone hydrochloride; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; at 120 ℃; for 48h; under 7600.51 Torr; Autoclave;
DOI:10.1021/acs.orglett.8b00538