C₄₂H₅₀O₁₆

Base Information

• Chemical Name: C₄₂H₅₀O₁₆
• CAS No.: 1160725-25-6
• Molecular Formula: C₄₂H₅₀O₁₆
• Molecular Weight: 810.849
• Mol file: 1160725-25-6.mol

Synonyms:C₄₂H₅₀O₁₆

Chemical Property of C₄₂H₅₀O₁₆

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₄₂H₅₀O₁₆

There total 1 articles about C₄₂H₅₀O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(2S,3S)-2,3-dimethoxy-1,4-butanediol (24679-72-9) + 4-O-benzyl-3,5-di-O-(methoxymethyl)gallic acid (1034343-24-2) → C42H50O16 (1160725-25-6)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere;

DOI:10.1021/jo201750d

Reference yield: 100.0%

C42H50O16 (1160725-25-6) → (2S,3S)-2,3-dimethoxy-1,4-butandiyl bis(4-O-benzylgallate) (1160725-26-7)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; isopropyl alcohol; at 50 - 60 ℃; for 32h;

DOI:10.1021/jo201750d

Reference yield:

C42H50O16 (1160725-25-6) → (2S,3S)-2,3-dimethoxy-1,4-butandiyl 5,5'-bis(benzyloxy)-4,4',6,6'-tetrahydroxy-1,1'-biphenyl-2,2'-dicarboxylate

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride / tetrahydrofuran; water; isopropyl alcohol / 32 h / 50 - 60 °C

2: N-butylamine; copper dichloride / methanol / 0.5 h / 20 °C

With hydrogenchloride; N-butylamine; copper dichloride; In tetrahydrofuran; methanol; water; isopropyl alcohol;

DOI:10.1021/jo201750d

upstream raw materials:

(2S,3S)-2,3-dimethoxy-1,4-butanediol

4-O-benzyl-3,5-di-O-(methoxymethyl)gallic acid

Downstream raw materials:

(2S,3S)-2,3-dimethoxy-1,4-butandiyl bis(4-O-benzylgallate)