2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-2,2-dimethyl-6-((1-phenyl-1H-tetrazol-5-ylsulfonyl)methyl)-1,3-dioxan-4-yl)acetate

Base Information

Chemical Name:2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-2,2-dimethyl-6-((1-phenyl-1H-tetrazol-5-ylsulfonyl)methyl)-1,3-dioxan-4-yl)acetate
CAS No.:1257341-69-7
Molecular Formula:C₂₆H₃₂N₄O₆S
Molecular Weight:528.629
Hs Code.:

Synonyms:2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-2,2-dimethyl-6-((1-phenyl-1H-tetrazol-5-ylsulfonyl)methyl)-1,3-dioxan-4-yl)acetate

Suppliers and Price of 2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-2,2-dimethyl-6-((1-phenyl-1H-tetrazol-5-ylsulfonyl)methyl)-1,3-dioxan-4-yl)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-2,2-dimethyl-6-((1-phenyl-1H-tetrazol-5-ylsulfonyl)methyl)-1,3-dioxan-4-yl)acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-2,2-dimethyl-6-((1-phenyl-1H-tetrazol-5-ylsulfonyl)methyl)-1,3-dioxan-4-yl)acetate

There total 7 articles about 2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-2,2-dimethyl-6-((1-phenyl-1H-tetrazol-5-ylsulfonyl)methyl)-1,3-dioxan-4-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1257341-65-3
2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-2,2-dimethyl-6-((1-phenyl-1H-tetrazol-5-ylthio)methyl)-1,3-dioxan-4-yl)acetate

: 1257341-69-7
2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-2,2-dimethyl-6-((1-phenyl-1H-tetrazol-5-ylsulfonyl)methyl)-1,3-dioxan-4-yl)acetate

Guidance literature:: With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In di-iso-propyl alcohol; at 0 - 20 ℃; for 30h;

Reference yield:

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1257341-69-7
2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-2,2-dimethyl-6-((1-phenyl-1H-tetrazol-5-ylsulfonyl)methyl)-1,3-dioxan-4-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate / methanol / 1 h / 0 - 20 °C

2: N,N-dimethyl-formamide / 24 h / 90 °C

3: dihydrogen peroxide; hexaammonium heptamolybdate tetrahydrate / di-iso-propyl alcohol / 30 h / 0 - 20 °C

With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; sodium methylate; In methanol; di-iso-propyl alcohol; N,N-dimethyl-formamide;

Reference yield:

: 151-05-3
1,1-dimethyl-2-phenylethyl acetate

: 1257341-69-7
2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-2,2-dimethyl-6-((1-phenyl-1H-tetrazol-5-ylsulfonyl)methyl)-1,3-dioxan-4-yl)acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1.67 h / -75 °C / Inert atmosphere

1.2: 5.33 h / 0 °C / Inert atmosphere

2.1: diethyl methoxy borane / tetrahydrofuran; methanol / 1 h / -75 °C

2.2: 5 h

2.3: 0.5 h

3.1: methanesulfonic acid / acetone / 2 h / 20 °C

4.1: N,N-dimethyl-formamide / 24 h / 90 °C

5.1: dihydrogen peroxide; hexaammonium heptamolybdate tetrahydrate / di-iso-propyl alcohol / 30 h / 0 - 20 °C

With methanesulfonic acid; hexaammonium heptamolybdate tetrahydrate; diethyl methoxy borane; dihydrogen peroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; di-iso-propyl alcohol; N,N-dimethyl-formamide; acetone;