H-δ-Ava-Phe-Phe-Gly-Leu-Nle-NH2

Base Information

Chemical Name:H-δ-Ava-Phe-Phe-Gly-Leu-Nle-NH2
CAS No.:123622-31-1
Molecular Formula:C₃₇H₅₅N₇O₆
Molecular Weight:693.887
Hs Code.:

Synonyms:H-δ-Ava-Phe-Phe-Gly-Leu-Nle-NH2

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Chemical Property of H-δ-Ava-Phe-Phe-Gly-Leu-Nle-NH2

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Technology Process of H-δ-Ava-Phe-Phe-Gly-Leu-Nle-NH2

There total 17 articles about H-δ-Ava-Phe-Phe-Gly-Leu-Nle-NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35661-40-6
N-Fmoc L-Phe

: 123622-31-1
H-δ-Ava-Phe-Phe-Gly-Leu-Nle-NH2

Guidance literature:: Multi-step reaction with 8 steps

1: SOCl₂ / CH₂Cl₂ / 0.5 h / Heating

2: 5percent Na₂CO₃ / CHCl₃ / 0.17 h

3: 4-(aminomethyl)-piperidine (4-AMP) / CHCl₃ / 0.5 h

4: 5percent Na₂CO₃ / CHCl₃ / 0.17 h

5: 4-(aminomethyl)-piperidine (4-AMP) / CHCl₃ / 0.5 h

6: 5percent Na₂CO₃ / CHCl₃ / 0.17 h

7: 4-(aminomethyl)-piperidine (4-AMP) / CHCl₃ / 0.5 h

8: 15percent NH₃ / methanol / 40 h / Ambient temperature

With ammonium hydroxide; thionyl chloride; sodium carbonate; 4-Aminomethylpiperidine; In methanol; dichloromethane; chloroform;
DOI:10.1021/jo00289a056

Reference yield:

: 103321-57-9
2S-flouren-9-ylmethoxycarbonylamino-3-phenylpropionyl chloride

: 123622-31-1
H-δ-Ava-Phe-Phe-Gly-Leu-Nle-NH2

Guidance literature:: Multi-step reaction with 7 steps

1: 5percent Na₂CO₃ / CHCl₃ / 0.17 h

2: 4-(aminomethyl)-piperidine (4-AMP) / CHCl₃ / 0.5 h

3: 5percent Na₂CO₃ / CHCl₃ / 0.17 h

4: 4-(aminomethyl)-piperidine (4-AMP) / CHCl₃ / 0.5 h

5: 5percent Na₂CO₃ / CHCl₃ / 0.17 h

6: 4-(aminomethyl)-piperidine (4-AMP) / CHCl₃ / 0.5 h

7: 15percent NH₃ / methanol / 40 h / Ambient temperature

With ammonium hydroxide; sodium carbonate; 4-Aminomethylpiperidine; In methanol; chloroform;
DOI:10.1021/jo00289a056