C₁₆H₁₉BrClNO₃

Base Information

Chemical Name:C₁₆H₁₉BrClNO₃
CAS No.:1432502-42-5
Molecular Formula:C₁₆H₁₉BrClNO₃
Molecular Weight:388.689
Hs Code.:

C<sub>16</sub>H<sub>19</sub>BrClNO<sub>3</sub>

Synonyms:C₁₆H₁₉BrClNO₃

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Chemical Property of C₁₆H₁₉BrClNO₃

Chemical Property:

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Technology Process of C₁₆H₁₉BrClNO₃

There total 12 articles about C₁₆H₁₉BrClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1432502-41-4
C₁₆H₁₉BrClNO₂

: 1432502-42-5
C₁₆H₁₉BrClNO₃

Guidance literature:: C₁₆H₁₉BrClNO₂; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

With (+)-[(8,8-dichlorocamphoryl)sulfonyl]oxaziridine; In tetrahydrofuran; at -78 ℃;

Reference yield:

: 1432502-36-7
C₁₄H₁₇BrClNO₄

: 1432502-42-5
C₁₆H₁₉BrClNO₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: dmap / dichloromethane / 0.17 h / -5 °C / Inert atmosphere

1.2: -5 - 20 °C

2.1: acetic acid / dichloromethane / 0.17 h / 0 °C

2.2: 1 h / 0 °C

3.1: toluene / 2 h / Reflux

4.1: trifluoroacetic acid / dichloromethane / 4 h / 0 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C / Inert atmosphere

5.2: 2 h

6.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere

6.2: -78 °C

With dmap; sodium hexamethyldisilazane; sodium hydride; acetic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; toluene; mineral oil;

Reference yield:

: 1213929-66-8,444727-07-5
C₉H₉BrClNO₂

: 1432502-42-5
C₁₆H₁₉BrClNO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydroxide / water; acetonitrile / 0 - 20 °C

2.1: dmap / dichloromethane / 0.17 h / -5 °C / Inert atmosphere

2.2: -5 - 20 °C

3.1: acetic acid / dichloromethane / 0.17 h / 0 °C

3.2: 1 h / 0 °C

4.1: toluene / 2 h / Reflux

5.1: trifluoroacetic acid / dichloromethane / 4 h / 0 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C / Inert atmosphere

6.2: 2 h

7.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere

7.2: -78 °C

With dmap; sodium hexamethyldisilazane; sodium hydride; acetic acid; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile; mineral oil;