Technology Process of [(3,5-diphenyl-2-(2-piridyl)pyrrolide)Pt(C2H4)Cl]
There total 1 articles about [(3,5-diphenyl-2-(2-piridyl)pyrrolide)Pt(C2H4)Cl] which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hexamethyldisilazane;
In
tetrahydrofuran;
byproducts: LiCl; (N2); std. Schlenk technique; Li compd. was added to soln. of ligand (1 equiv.) in THF; stirred for 30 min; soln. of Pt complex (0.5 equiv.) in THF was added; stirred for 1 h; evapd. (vac.); dissolved in toluene; filtered through Celite; evapd. (vac.); washed (pentane); elem. anal.;
DOI:10.1021/om9002686
- Guidance literature:
-
In
benzene;
(N2); std. Schlenk technique; HSiEt3 (4 equiv.) was added to soln. of ptcomplex in C6H6; stirred for 12 h; evapd. (vac.); dissolved in pentane; slowly evapd.; elem. anal.;
DOI:10.1021/om9002686
- Guidance literature:
-
In
benzene;
(N2); std. Schlenk technique; HSiEtMe2 (4 equiv.) was added to soln. of Pt complex in C6H6; stirred for 12 h; evapd. (vac.); dissolved in THF/pentane (1/1); concd.; slowly evapd.; elem. anal.;
DOI:10.1021/om9002686
