tert-butyl {2-[1-(4-chlorophenyl)cyclobutyl]-2-(3-formylphenyl)ethyl}carbamate

Base Information

Chemical Name:tert-butyl {2-[1-(4-chlorophenyl)cyclobutyl]-2-(3-formylphenyl)ethyl}carbamate
CAS No.:1359840-95-1
Molecular Formula:C₂₄H₂₈ClNO₃
Molecular Weight:413.944
Hs Code.:

Synonyms:tert-butyl {2-[1-(4-chlorophenyl)cyclobutyl]-2-(3-formylphenyl)ethyl}carbamate

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Chemical Property of tert-butyl {2-[1-(4-chlorophenyl)cyclobutyl]-2-(3-formylphenyl)ethyl}carbamate

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Technology Process of tert-butyl {2-[1-(4-chlorophenyl)cyclobutyl]-2-(3-formylphenyl)ethyl}carbamate

There total 6 articles about tert-butyl {2-[1-(4-chlorophenyl)cyclobutyl]-2-(3-formylphenyl)ethyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1359840-94-0
tert-butyl {2-[1-(4-chlorophenyl)cyclobutyl]-2-(3-cyanophenyl)ethyl}carbamate

: 1359840-95-1
tert-butyl {2-[1-(4-chlorophenyl)cyclobutyl]-2-(3-formylphenyl)ethyl}carbamate

Guidance literature:: tert-butyl {2-[1-(4-chlorophenyl)cyclobutyl]-2-(3-cyanophenyl)ethyl}carbamate; With diisobutylaluminium hydride; In toluene; at -78 ℃; for 2h;

With hydrogenchloride; water; In toluene;

With sodium hydrogencarbonate; In water;

Reference yield:

: 106079-12-3
1-(4-chlorophenyl)-cyclobutanecarboxaldehyde

: 1359840-95-1
tert-butyl {2-[1-(4-chlorophenyl)cyclobutyl]-2-(3-formylphenyl)ethyl}carbamate

Guidance literature:: Multi-step reaction with 6 steps

1: potassium tert-butylate / tert-butyl alcohol; tetrahydrofuran / 20 °C

2: triethylamine; trifluoroacetic anhydride / dichloromethane / 0 - 20 °C

3: isopropylmagnesium chloride / tetrahydrofuran / 0.42 h / -30 °C

4: zinc; acetic acid / tetrahydrofuran / 2 h / 20 °C

5: N-ethyl-N,N-diisopropylamine / acetonitrile / 5 h / 60 °C

6: diisobutylaluminium hydride / toluene / 2 h / -78 °C

With potassium tert-butylate; isopropylmagnesium chloride; diisobutylaluminium hydride; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; zinc; In tetrahydrofuran; dichloromethane; toluene; acetonitrile; tert-butyl alcohol;

Reference yield:

: 1359840-92-8
3-{1-[1-(4-chlorophenyl)cyclobutyl]-2-nitroethyl}benzonitrile

: 1359840-95-1
tert-butyl {2-[1-(4-chlorophenyl)cyclobutyl]-2-(3-formylphenyl)ethyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: zinc; acetic acid / tetrahydrofuran / 2 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / acetonitrile / 5 h / 60 °C

3: diisobutylaluminium hydride / toluene / 2 h / -78 °C

With diisobutylaluminium hydride; acetic acid; N-ethyl-N,N-diisopropylamine; zinc; In tetrahydrofuran; toluene; acetonitrile;