1-Phenyl-3,6-heptandion-bis

Base Information

Chemical Name:1-Phenyl-3,6-heptandion-bis
CAS No.:87378-02-7
Molecular Formula:C₁₅H₂₂N₂O₂
Molecular Weight:262.352
Hs Code.:

1-Phenyl-3,6-heptandion-bis<O-methyloxim>

Synonyms:1-Phenyl-3,6-heptandion-bis

Suppliers and Price of 1-Phenyl-3,6-heptandion-bis

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Phenyl-3,6-heptandion-bis

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Technology Process of 1-Phenyl-3,6-heptandion-bis

There total 2 articles about 1-Phenyl-3,6-heptandion-bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87377-95-5
(Z,Z)-<2,5-hexanedione bis(O-methyloxime)>

: 87378-02-7
1-Phenyl-3,6-heptandion-bis

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 0.5 h / 170 °C

2: 1.) n-BuLi / 1.) THF, Hexan, 2 min, -65 deg C, 2.) 6 min, -65 deg C

With n-butyllithium;
DOI:10.1055/s-1983-30441

Reference yield:

: 100-39-0
benzyl bromide

: 87377-96-6
2,5-Hexandion-2(E),5(E)-bis

: 87378-02-7
1-Phenyl-3,6-heptandion-bis

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF, Hexan, 2 min, -65 deg C, 2.) 6 min, -65 deg C;
DOI:10.1055/s-1983-30441