Ethenamine, N,N-dimethyl-2-5-nitro-2,6-bis(phenylmethoxy)-4-pyrimidinyl-

Base Information

Chemical Name:Ethenamine, N,N-dimethyl-2-5-nitro-2,6-bis(phenylmethoxy)-4-pyrimidinyl-
CAS No.:222631-55-2
Molecular Formula:C₂₂H₂₂N₄O₄
Molecular Weight:406.441
Hs Code.:

Synonyms:Ethenamine, N,N-dimethyl-2-5-nitro-2,6-bis(phenylmethoxy)-4-pyrimidinyl-

Suppliers and Price of Ethenamine, N,N-dimethyl-2-5-nitro-2,6-bis(phenylmethoxy)-4-pyrimidinyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Ethenamine, N,N-dimethyl-2-5-nitro-2,6-bis(phenylmethoxy)-4-pyrimidinyl-

Chemical Property:

PSA：93.30000
LogP:4.59830

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethenamine, N,N-dimethyl-2-5-nitro-2,6-bis(phenylmethoxy)-4-pyrimidinyl-

There total 1 articles about Ethenamine, N,N-dimethyl-2-5-nitro-2,6-bis(phenylmethoxy)-4-pyrimidinyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 30958-38-4
2,4-bis-O-benzyl-6-methyl-5-nitro pyrimidine

: 222631-55-2
2,4-bis-O-benzyl-5-nitro-6-β-dimethylaminovinylpyrimidine

Guidance literature:: In N,N-dimethyl-formamide; at 60 - 65 ℃; Inert atmosphere;

Reference yield:

: 222631-55-2
2,4-bis-O-benzyl-5-nitro-6-β-dimethylaminovinylpyrimidine

: 1446175-09-2
2,4-bis-benzyloxy-5-N-boc-7-iodopyrrolo[3,2-d]pyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; zinc / 20 °C

2: N-iodo-succinimide / dichloromethane / 20 °C / Inert atmosphere

3: dmap / tetrahydrofuran / 1 h

With dmap; N-iodo-succinimide; acetic acid; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmc.2015.06.025

Reference yield:

: 222631-55-2
2,4-bis-O-benzyl-5-nitro-6-β-dimethylaminovinylpyrimidine

: 1446175-04-7
7-iodo-2,4-bis-benzyloxy-5H-pyrrolo[3,2-d]-pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; zinc / 20 °C

2: N-iodo-succinimide / dichloromethane / 20 °C / Inert atmosphere

With N-iodo-succinimide; acetic acid; zinc; In dichloromethane;
DOI:10.1016/j.bmc.2015.06.025