2-methylene-N-phenyl-3-(phenylsulfonyl)-4-<(trimethylsilyl)oxy>tridecanamide

Base Information

Chemical Name:2-methylene-N-phenyl-3-(phenylsulfonyl)-4-<(trimethylsilyl)oxy>tridecanamide
CAS No.:118336-42-8
Molecular Formula:C₂₉H₄₃NO₄SSi
Molecular Weight:529.816
Hs Code.:

Synonyms:2-methylene-N-phenyl-3-(phenylsulfonyl)-4-<(trimethylsilyl)oxy>tridecanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methylene-N-phenyl-3-(phenylsulfonyl)-4-<(trimethylsilyl)oxy>tridecanamide

Chemical Property:

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Technology Process of 2-methylene-N-phenyl-3-(phenylsulfonyl)-4-<(trimethylsilyl)oxy>tridecanamide

There total 3 articles about 2-methylene-N-phenyl-3-(phenylsulfonyl)-4-<(trimethylsilyl)oxy>tridecanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 75-77-4
chloro-trimethyl-silane

: 111947-53-6
4-hydroxy-2-methylene-N-phenyl-3-(phenylsulfonyl)tridecanamide

: 118336-42-8
2-methylene-N-phenyl-3-(phenylsulfonyl)-4-<(trimethylsilyl)oxy>tridecanamide

Guidance literature:: DOI:10.1021/jo00262a020

Reference yield:

: 112-31-2
caprinaldehyde

: 118336-42-8
2-methylene-N-phenyl-3-(phenylsulfonyl)-4-<(trimethylsilyl)oxy>tridecanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, HMPA, -78 deg C, 1 h, 2.) -78 deg C, 2 h

2: 89 percent

With n-butyllithium;
DOI:10.1021/jo00262a020

Reference yield:

: 87504-85-6
N-phenyl-2-<(phenylsulfonyl)methyl>propenamide

: 118336-42-8
2-methylene-N-phenyl-3-(phenylsulfonyl)-4-<(trimethylsilyl)oxy>tridecanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, HMPA, -78 deg C, 1 h, 2.) -78 deg C, 2 h

2: 89 percent

With n-butyllithium;
DOI:10.1021/jo00262a020