2,6-dichloro-3-(4-chlorophenyl)-4-((4-methoxyphenyl)sulfinyl)pyridine

Base Information

Chemical Name:2,6-dichloro-3-(4-chlorophenyl)-4-((4-methoxyphenyl)sulfinyl)pyridine
CAS No.:1309446-68-1
Molecular Formula:C₁₈H₁₂Cl₃NO₂S
Molecular Weight:412.724
Hs Code.:

Synonyms:2,6-dichloro-3-(4-chlorophenyl)-4-((4-methoxyphenyl)sulfinyl)pyridine

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Chemical Property of 2,6-dichloro-3-(4-chlorophenyl)-4-((4-methoxyphenyl)sulfinyl)pyridine

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Technology Process of 2,6-dichloro-3-(4-chlorophenyl)-4-((4-methoxyphenyl)sulfinyl)pyridine

There total 2 articles about 2,6-dichloro-3-(4-chlorophenyl)-4-((4-methoxyphenyl)sulfinyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2,6-dichloropyridin-4-yl)magnesium chloride lithium chloridre

: 1309446-68-1
2,6-dichloro-3-(4-chlorophenyl)-4-((4-methoxyphenyl)sulfinyl)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / -20 - 25 °C / Inert atmosphere

2.1: 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex / tetrahydrofuran / -30 °C / Inert atmosphere

2.2: 25 °C / Inert atmosphere

2.3: 2 h / 50 °C / Inert atmosphere

With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; In tetrahydrofuran;
DOI:10.1002/chem.201003657

Reference yield:

: 31401-23-7
p-methoxybenzenesulfinyl chloride

: 1309446-68-1
2,6-dichloro-3-(4-chlorophenyl)-4-((4-methoxyphenyl)sulfinyl)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / -20 - 25 °C / Inert atmosphere

2.1: 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex / tetrahydrofuran / -30 °C / Inert atmosphere

2.2: 25 °C / Inert atmosphere

2.3: 2 h / 50 °C / Inert atmosphere

With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; In tetrahydrofuran;
DOI:10.1002/chem.201003657

Reference yield: 61.0%

: 636-98-6
p-nitrobenzene iodide

: 1309446-68-1
2,6-dichloro-3-(4-chlorophenyl)-4-((4-methoxyphenyl)sulfinyl)pyridine

: 1309446-73-8
2,6-dichloro-3-(4-chlorophenyl)-4-(4-nitrophenyl)pyridine

Guidance literature:: 2,6-dichloro-3-(4-chlorophenyl)-4-((4-methoxyphenyl)sulfinyl)pyridine; With isopropylmagnesium bromide; In 2-methyl-THF; at -50 ℃; for 0.0833333h; Inert atmosphere;

With zinc(II) chloride; In tetrahydrofuran; 2-methyl-THF; for 0.5h; Inert atmosphere;

p-nitrobenzene iodide; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 2-methyl-THF; at 50 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.201003657