N-[2,3-bis(4-methoxyphenyl)pyrido[3,4-b]pyrazin-8-yl]benzophenone imine

Base Information

Chemical Name:N-[2,3-bis(4-methoxyphenyl)pyrido[3,4-b]pyrazin-8-yl]benzophenone imine
CAS No.:1305317-10-5
Molecular Formula:C₃₄H₂₆N₄O₂
Molecular Weight:522.606
Hs Code.:

Synonyms:N-[2,3-bis(4-methoxyphenyl)pyrido[3,4-b]pyrazin-8-yl]benzophenone imine

Suppliers and Price of N-[2,3-bis(4-methoxyphenyl)pyrido[3,4-b]pyrazin-8-yl]benzophenone imine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[2,3-bis(4-methoxyphenyl)pyrido[3,4-b]pyrazin-8-yl]benzophenone imine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[2,3-bis(4-methoxyphenyl)pyrido[3,4-b]pyrazin-8-yl]benzophenone imine

There total 6 articles about N-[2,3-bis(4-methoxyphenyl)pyrido[3,4-b]pyrazin-8-yl]benzophenone imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1013-88-3
Benzophenone imine

: 1305317-08-1
8-bromo-2,3-bis(4-methoxyphenyl)pyrido[3,4-b]pyrazine

: 1305317-10-5
N-[2,3-bis(4-methoxyphenyl)pyrido[3,4-b]pyrazin-8-yl]benzophenone imine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; rac-BINAP; sodium t-butanolate; In toluene; at 100 ℃; Inert atmosphere;
DOI:10.1055/s-0030-1259429

Reference yield:

: 504-24-5
4-aminopyridine

: 1305317-10-5
N-[2,3-bis(4-methoxyphenyl)pyrido[3,4-b]pyrazin-8-yl]benzophenone imine

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid; nitric acid / 5.5 h / 10 - 20 °C

2.1: sulfuric acid / 20 - 90 °C

3.1: potassium acetate; acetic acid / 1 h / 20 °C

3.2: 20 °C

4.1: water; tin(ll) chloride / ethanol / 2 h / Reflux

5.1: 1,4-dioxane / Reflux

6.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; rac-BINAP; sodium t-butanolate / toluene / 100 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; rac-BINAP; sulfuric acid; water; nitric acid; potassium acetate; acetic acid; tin(ll) chloride; sodium t-butanolate; In 1,4-dioxane; ethanol; toluene; 6.1: Buchwald reaction;
DOI:10.1055/s-0030-1259429

Reference yield:

: 4635-08-9
3,4-diamino-5-bromopyridine

: 1305317-10-5
N-[2,3-bis(4-methoxyphenyl)pyrido[3,4-b]pyrazin-8-yl]benzophenone imine

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-dioxane / Reflux

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; rac-BINAP; sodium t-butanolate / toluene / 100 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; rac-BINAP; sodium t-butanolate; In 1,4-dioxane; toluene; 2: Buchwald reaction;
DOI:10.1055/s-0030-1259429