(E,E)-4-[4-(3,4,5-tris{methyltetraethyleneoxy})styryl]-2,5-[bis[(S)-2-methylbutoxy]styryl]phenylnitrile

Base Information

Chemical Name:(E,E)-4-[4-(3,4,5-tris{methyltetraethyleneoxy})styryl]-2,5-[bis[(S)-2-methylbutoxy]styryl]phenylnitrile
CAS No.:941579-68-6
Molecular Formula:C₆₀H₉₁NO₁₇
Molecular Weight:1098.38
Hs Code.:

Synonyms:(E,E)-4-[4-(3,4,5-tris{methyltetraethyleneoxy})styryl]-2,5-[bis[(S)-2-methylbutoxy]styryl]phenylnitrile

Suppliers and Price of (E,E)-4-[4-(3,4,5-tris{methyltetraethyleneoxy})styryl]-2,5-[bis[(S)-2-methylbutoxy]styryl]phenylnitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E,E)-4-[4-(3,4,5-tris{methyltetraethyleneoxy})styryl]-2,5-[bis[(S)-2-methylbutoxy]styryl]phenylnitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E,E)-4-[4-(3,4,5-tris{methyltetraethyleneoxy})styryl]-2,5-[bis[(S)-2-methylbutoxy]styryl]phenylnitrile

There total 4 articles about (E,E)-4-[4-(3,4,5-tris{methyltetraethyleneoxy})styryl]-2,5-[bis[(S)-2-methylbutoxy]styryl]phenylnitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 941579-66-4
(E)-4-[4-formyl-2,5-bis[(S)-2-methylbutoxy]styryl]phenylnitrile

: 941579-67-5
diethyl (3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl)phosphonate

: 941579-68-6
(E,E)-4-[4-(3,4,5-tris{methyltetraethyleneoxy})styryl]-2,5-[bis[(S)-2-methylbutoxy]styryl]phenylnitrile

Guidance literature:: diethyl (3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl)phosphonate; With potassium tert-butylate; In N,N-dimethyl-formamide; for 0.25h;

(E)-4-[4-formyl-2,5-bis[(S)-2-methylbutoxy]styryl]phenylnitrile; In N,N-dimethyl-formamide; at 20 ℃;

With iodine; In toluene; Further stages.; Heating;
DOI:10.1021/ja0711967

Reference yield:

: 1552-41-6
diethyl [(4-cyanophenyl)methyl]phosphonate

: 941579-68-6
(E,E)-4-[4-(3,4,5-tris{methyltetraethyleneoxy})styryl]-2,5-[bis[(S)-2-methylbutoxy]styryl]phenylnitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: 52 percent / potassium tert-butoxide / dimethylformamide / 2 h / 20 °C

2.1: potassium tert-butoxide / dimethylformamide / 0.25 h

2.2: dimethylformamide / 20 °C

2.3: 266 mg / iodine / toluene / Heating

With potassium tert-butylate; In N,N-dimethyl-formamide; 1.1: Wittig-Horner reaction / 2.2: Wittig-Horner reaction;
DOI:10.1021/ja0711967

Reference yield:

: 484046-58-4
3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl chloride

: 941579-68-6
(E,E)-4-[4-(3,4,5-tris{methyltetraethyleneoxy})styryl]-2,5-[bis[(S)-2-methylbutoxy]styryl]phenylnitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: 8 h / 160 °C

2.1: potassium tert-butoxide / dimethylformamide / 0.25 h

2.2: dimethylformamide / 20 °C

2.3: 266 mg / iodine / toluene / Heating

With potassium tert-butylate; In N,N-dimethyl-formamide; 1.1: Arbuzov reaction / 2.2: Wittig-Horner reaction;
DOI:10.1021/ja0711967