N-phenylthiocarbamoylacetamidine

Base Information

• Chemical Name: N-phenylthiocarbamoylacetamidine
• CAS No.: 98949-67-8
• Molecular Formula: C₉H₁₁N₃S
• Molecular Weight: 193.272

Synonyms:N-phenylthiocarbamoylacetamidine

Chemical Property of N-phenylthiocarbamoylacetamidine

Chemical Property:

Purity/Quality:

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Technology Process of N-phenylthiocarbamoylacetamidine

There total 3 articles about N-phenylthiocarbamoylacetamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

acetamidine hydrochloride (124-42-5) + phenyl isothiocyanate (103-72-0) → N-phenylthiocarbamoylacetamidine (98949-67-8)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; water; at 0 ℃;

DOI:10.1021/jo0009447

Reference yield: 31.0%

acetamidine hydrochloride (124-42-5) + phenyl isothiocyanate (103-72-0) → N-(phenylcarbamothioyl)acetimidamide (98949-67-8)

Guidance literature:

With potassium hydroxide; In methanol; at 20 ℃; for 0.5h;

DOI:10.1016/j.tet.2014.09.023

Reference yield:

phenyl isothiocyanate (103-72-0) + acetamidine (143-37-3) → N-(phenylcarbamothioyl)acetimidamide (98949-67-8)

Guidance literature:

With potassium carbonate; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1002/ejoc.201801642

upstream raw materials:

acetamidine hydrochloride

phenyl isothiocyanate

acetamidine

Downstream raw materials:

ethyl 4-methyl-2-(phenylamino)thiazole-5-carboxylate

3-methyl-5-(methylsulfanyl)-1-phenyl-1,2,4-triazole

3-methyl-N-phenyl-1,2,4-thiadiazol-5-amine

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