2-(3,5-dichloro-4-(2,2,2-trifluoroethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(3,5-dichloro-4-(2,2,2-trifluoroethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1437779-78-6
Molecular Formula:C₁₄H₁₆BCl₂F₃O₃
Molecular Weight:370.991
Hs Code.:

Synonyms:2-(3,5-dichloro-4-(2,2,2-trifluoroethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-(3,5-dichloro-4-(2,2,2-trifluoroethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-(3,5-dichloro-4-(2,2,2-trifluoroethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 5 articles about 2-(3,5-dichloro-4-(2,2,2-trifluoroethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.2%

: 1437779-77-5
1,3-dichloro-2-(2,2,2-trifluoroethoxy)benzene

: 73183-34-3
bis(pinacol)diborane

: 1437779-78-6
2-(3,5-dichloro-4-(2,2,2-trifluoroethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; 2-(((2,6-diisopropylphenyl)imino)methyl)pyridine; In n-heptane; for 3h; Reflux;

Reference yield:

: 57946-62-0
3,5-dichloro-4-(2,2,2-trifluoroethoxy)aniline

: 1437779-78-6
2-(3,5-dichloro-4-(2,2,2-trifluoroethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1: isopentyl nitrite / tetrahydrofuran / 6 h / Reflux

2: 2-(((2,6-diisopropylphenyl)imino)methyl)pyridine; bis(1,5-cyclooctadiene)diiridium(I) dichloride / n-heptane / 3 h / Reflux

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; 2-(((2,6-diisopropylphenyl)imino)methyl)pyridine; isopentyl nitrite; In tetrahydrofuran; n-heptane;

Reference yield:

: 99-30-9
4-nitro-2,6-dichloroaniline

: 1437779-78-6
2-(3,5-dichloro-4-(2,2,2-trifluoroethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride; sodium nitrite / water / 0 °C

2: ethyl 2-oxocyclohexane carboxylate; caesium carbonate; copper(I) bromide / dimethyl sulfoxide / 18 h / 80 °C / Inert atmosphere

3: hydrogenchloride; tin(ll) chloride / water; methanol / 20 °C

4: isopentyl nitrite / tetrahydrofuran / 6 h / Reflux

5: 2-(((2,6-diisopropylphenyl)imino)methyl)pyridine; bis(1,5-cyclooctadiene)diiridium(I) dichloride / n-heptane / 3 h / Reflux

With hydrogenchloride; bis(1,5-cyclooctadiene)diiridium(I) dichloride; caesium carbonate; ethyl 2-oxocyclohexane carboxylate; 2-(((2,6-diisopropylphenyl)imino)methyl)pyridine; tin(ll) chloride; copper(I) bromide; sodium nitrite; isopentyl nitrite; In tetrahydrofuran; methanol; n-heptane; water; dimethyl sulfoxide;