cis-1-chloroformyl-2-(4-methoxyphenyl)-6-methoxy-1,2,3,4-tetrahydronaphthalene

Base Information

Chemical Name:cis-1-chloroformyl-2-(4-methoxyphenyl)-6-methoxy-1,2,3,4-tetrahydronaphthalene
CAS No.:128237-20-7
Molecular Formula:C₁₉H₁₉ClO₃
Molecular Weight:330.811
Hs Code.:

Synonyms:cis-1-chloroformyl-2-(4-methoxyphenyl)-6-methoxy-1,2,3,4-tetrahydronaphthalene

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Chemical Property of cis-1-chloroformyl-2-(4-methoxyphenyl)-6-methoxy-1,2,3,4-tetrahydronaphthalene

Chemical Property:

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Technology Process of cis-1-chloroformyl-2-(4-methoxyphenyl)-6-methoxy-1,2,3,4-tetrahydronaphthalene

There total 5 articles about cis-1-chloroformyl-2-(4-methoxyphenyl)-6-methoxy-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: cis-1-carboxy-2-(4-methoxyphenyl)-6-methoxy-1,2,3,4-tetrahydronaphthalene

: 128237-20-7
cis-1-chloroformyl-2-(4-methoxyphenyl)-6-methoxy-1,2,3,4-tetrahydronaphthalene

Guidance literature:: With oxalyl dichloride; In N,N-dimethyl-formamide; at -20 ℃; for 2h;
DOI:10.1039/c39900000518

Reference yield:

: 56437-05-9
1-cyano-4-methoxybenzocyclobutane

: 128237-20-7
cis-1-chloroformyl-2-(4-methoxyphenyl)-6-methoxy-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / 0.75 h / 175 °C

2: 29 percent / KOH / ethane-1,2-diol / 12 h / 180 °C

3: (COCl)2, DMF

With potassium hydroxide; oxalyl dichloride; N,N-dimethyl-formamide; In ethylene glycol;

Reference yield:

: 96045-14-6,118602-04-3,128237-19-4
cis-1-cyano-2-(4-methoxyphenyl)-6-methoxy-1,2,3,4-tetrahydronaphthalene

: 128237-20-7
cis-1-chloroformyl-2-(4-methoxyphenyl)-6-methoxy-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / KOH / ethane-1,2-diol / 12 h / 180 °C

2: (COCl)2, DMF

With potassium hydroxide; oxalyl dichloride; N,N-dimethyl-formamide; In ethylene glycol;