(4R,5R)-1-(2-(4,5-bis(hydroxydiphenylmethyl)-2-methyl-1,3-dioxolan-2-yl)ethyl)-3-methyl-1H-imidazol-3-ium tetrafluoroborate

Base Information

Chemical Name:(4R,5R)-1-(2-(4,5-bis(hydroxydiphenylmethyl)-2-methyl-1,3-dioxolan-2-yl)ethyl)-3-methyl-1H-imidazol-3-ium tetrafluoroborate
CAS No.:1372101-04-6
Molecular Formula:BF₄*C₃₆H₃₇N₂O₄
Molecular Weight:648.505
Hs Code.:

Synonyms:(4R,5R)-1-(2-(4,5-bis(hydroxydiphenylmethyl)-2-methyl-1,3-dioxolan-2-yl)ethyl)-3-methyl-1H-imidazol-3-ium tetrafluoroborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,5R)-1-(2-(4,5-bis(hydroxydiphenylmethyl)-2-methyl-1,3-dioxolan-2-yl)ethyl)-3-methyl-1H-imidazol-3-ium tetrafluoroborate

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Technology Process of (4R,5R)-1-(2-(4,5-bis(hydroxydiphenylmethyl)-2-methyl-1,3-dioxolan-2-yl)ethyl)-3-methyl-1H-imidazol-3-ium tetrafluoroborate

There total 4 articles about (4R,5R)-1-(2-(4,5-bis(hydroxydiphenylmethyl)-2-methyl-1,3-dioxolan-2-yl)ethyl)-3-methyl-1H-imidazol-3-ium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 14104-20-2
silver tetrafluoroborate

: 1370590-40-1
(4R,5R)-1-(2-(4,5-bis(hydroxydiphenylmethyl)-2-methyl-1,3-dioxolan-2-yl)ethyl)-3-methyl-1H-imidazol-3-ium iodide

: 1372101-04-6
(4R,5R)-1-(2-(4,5-bis(hydroxydiphenylmethyl)-2-methyl-1,3-dioxolan-2-yl)ethyl)-3-methyl-1H-imidazol-3-ium tetrafluoroborate

Guidance literature:: In acetonitrile; at 20 ℃; for 1h;
DOI:10.3998/ark.5550190.0013.322

Reference yield:

: 1370590-38-7
(4R,5R)-2-(2-(1H-imidazol-1-yl)ethyl)-2-methyl-1,3-dioxolane-4,5-dicarboxylate dimethyl ester

: 1372101-04-6
(4R,5R)-1-(2-(4,5-bis(hydroxydiphenylmethyl)-2-methyl-1,3-dioxolan-2-yl)ethyl)-3-methyl-1H-imidazol-3-ium tetrafluoroborate

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium / tetrahydrofuran / Reflux

1.2: 24 h / -15 - 20 °C

2.1: acetonitrile / Inert atmosphere; Reflux

3.1: acetonitrile / 1 h / 20 °C

With magnesium; In tetrahydrofuran; acetonitrile; 1.2: |Grignard Reaction;
DOI:10.3998/ark.5550190.0013.322

Reference yield:

: 59543-81-6
4-(1H-imidazol-1-yl)-2-butanone

: 1372101-04-6
(4R,5R)-1-(2-(4,5-bis(hydroxydiphenylmethyl)-2-methyl-1,3-dioxolan-2-yl)ethyl)-3-methyl-1H-imidazol-3-ium tetrafluoroborate

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron trifluoride diethyl etherate / ethyl acetate / 20 °C

2.1: magnesium / tetrahydrofuran / Reflux

2.2: 24 h / -15 - 20 °C

3.1: acetonitrile / Inert atmosphere; Reflux

4.1: acetonitrile / 1 h / 20 °C

With boron trifluoride diethyl etherate; magnesium; In tetrahydrofuran; ethyl acetate; acetonitrile; 2.2: |Grignard Reaction;
DOI:10.3998/ark.5550190.0013.322