Technology Process of (E,Z)-7-phenyl-6-heptenal
There total 7 articles about (E,Z)-7-phenyl-6-heptenal which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetraethylammonium perchlorate;
In
N,N-dimethyl-formamide;
at 60 ℃;
Electrochemical reaction;
DOI:10.1021/jo001578u
- Guidance literature:
-
With
oxygen;
In
isopropyl alcohol;
for 0.333333h;
Product distribution;
UV-irradiation;
DOI:10.1246/bcsj.75.1223
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: NaH / dimethylsulfoxide / 65 °C
1.2: 20 °C
2.1: DCC; DMAP / CH2Cl2 / 2 h / 20 °C
3.1: 14 percent / tetraethylammonium perchlorate / dimethylformamide / 60 °C / Electrochemical reaction
With
dmap; tetraethylammonium perchlorate; sodium hydride; dicyclohexyl-carbodiimide;
In
dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jo001578u
