N-benzoyl-2-methoxy-o-anisamide

Base Information

• Chemical Name: N-benzoyl-2-methoxy-o-anisamide
• CAS No.: 92552-95-9
• Molecular Formula: C₁₅H₁₃NO₃
• Molecular Weight: 255.273
• Mol file: 92552-95-9.mol

Synonyms:N-benzoyl-2-methoxy-o-anisamide

Chemical Property of N-benzoyl-2-methoxy-o-anisamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-benzoyl-2-methoxy-o-anisamide

There total 8 articles about N-benzoyl-2-methoxy-o-anisamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

N-(2-methoxybenzyl)-benzoylamide (143572-98-9) → N-benzoyl-2-methoxy-o-anisamide (92552-95-9)

Guidance literature:

With tert.-butylhydroperoxide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; copper(I) bromide; In water; acetonitrile; at 20 ℃; for 8h;

DOI:10.1002/cjoc.201500190

Reference yield: 60.0%

2-methoxybenzamide (2439-77-2) + benzyl alcohol (100-51-6,185532-71-2) → N-benzoyl-2-methoxy-o-anisamide (92552-95-9)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; 9-azanoradamantane N-oxyl; potassium tert-butylate; oxygen; copper(l) chloride; In tetrahydrofuran; at 23 ℃; for 24h; Molecular sieve;

DOI:10.1039/c8sc01410h

Reference yield:

2-methoxybenzamide (2439-77-2) → N-benzoyl-2-methoxy-o-anisamide (92552-95-9)

Guidance literature:

With sodium amide; benzene; at 120 - 130 ℃; durch Behandeln mit Phenylbenzoat in Pyridin;

upstream raw materials:

diazomethane

N-benzoylsalicylamide

2-methoxybenzamide

methyl iodide

Downstream raw materials:

2-methoxybenzamide

benzoic acid