N-Benzoyl-2-hydroxybenzamide

Base Information

• Chemical Name: N-Benzoyl-2-hydroxybenzamide
• CAS No.: 5663-74-1
• Molecular Formula: C14H11NO3
• Molecular Weight: 241.246
• Mol file: 5663-74-1.mol

Synonyms:N-benzoyl-2-hydroxy-benzamide;N-Salicoyl-benzamid;N-benzoylsalicylamide;N-Benzoyl-salicylamid;benzoyl-salicyloyl-amine;Benzoyl-salicyloyl-amin;N-Benzoyl-salicylsaeureamid;Benzamide,N-benzoyl-2-hydroxy;

Chemical Property of N-Benzoyl-2-hydroxybenzamide

Chemical Property:

• Melting Point: 208 °C
• Boiling Point: 450.6±37.0 °C(Predicted)
• PKA: 7.98±0.30(Predicted)
• PSA: 69.89000
• Density: 1.36 g/cm3
• LogP: 2.53720

Purity/Quality:

99% ^*data from raw suppliers

N-BENZOYL-2-HYDROXYBENZAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-Benzoyl-2-hydroxybenzamide

There total 27 articles about N-Benzoyl-2-hydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Phenyl-2,3-dihydro-benzo[e][1,3]oxazin-4-one (6629-80-7) + phosphorus pentachloride (10026-13-8,874483-75-7) → N-benzoylsalicylamide (5663-74-1) + salicylonitrile (611-20-1) + 2-cyanophenyl benzoate (71365-79-2) + salicylamide (65-45-2)

Guidance literature:

at 140 ℃; Behandeln des Reaktionsprodukts mit Wasser oder konz. Schwefelsaeure;

Reference yield:

chloroform (67-66-3,8013-54-5) + 2-Phenyl-2,3-dihydro-benzo[e][1,3]oxazin-4-one (6629-80-7) + phosphorus pentachloride (10026-13-8,874483-75-7) → N-benzoylsalicylamide (5663-74-1) + salicylonitrile (611-20-1) + 2-cyanophenyl benzoate (71365-79-2) + salicylamide (65-45-2)

Guidance literature:

at 60 ℃; Behandeln des Reaktionsprodukts mit Wasser oder konz. Schwefelsaeure;

Reference yield:

pyridine (110-86-1) + dibenzoyl-(2-benzoyloxy-benzoyl)-amine (952008-51-4) → N-benzoylsalicylamide (5663-74-1) + benzoic acid (65-85-0,8013-63-6)

Guidance literature:

upstream raw materials:

pyridine

dibenzoyl-(2-benzoyloxy-benzoyl)-amine

benzoic acid anhydride

salicylamide

Downstream raw materials:

N-benzoyl-2-methoxy-o-anisamide

acetyl-(2-benzoyloxy-benzoyl)-amine

2-phenyl-4H-1,3-benzoxazin-4-one

2-cyanophenyl benzoate