(+/-)-2-phenylselenophenyacetaldehyde

Base Information

• Chemical Name: (+/-)-2-phenylselenophenyacetaldehyde
• CAS No.: 82737-11-9
• Molecular Formula: C₁₄H₁₂OSe
• Molecular Weight: 275.209

Synonyms:(+/-)-2-phenylselenophenyacetaldehyde

Chemical Property of (+/-)-2-phenylselenophenyacetaldehyde

Chemical Property:

Purity/Quality:

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Technology Process of (+/-)-2-phenylselenophenyacetaldehyde

There total 4 articles about (+/-)-2-phenylselenophenyacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

Phenylselenyl chloride (5707-04-0) + (E)/(Z)-β-Trimethylsiloxystyrene (57044-58-3) → diphenyl diselenide (1666-13-3) + (+/-)-2-phenylselenophenyacetaldehyde (82737-11-9)

Guidance literature:

In tetrahydrofuran; for 0.166667h;

DOI:10.1016/0040-4020(95)00532-D

Reference yield: 85.0%

phenylacetaldehyde (122-78-1) + N-(phenylselanyl)morpholine (82737-08-4) → (+/-)-2-phenylselenophenyacetaldehyde (82737-11-9)

Guidance literature:

at 35 ℃; for 0.0833333h;

DOI:10.1016/S0040-4039(00)87157-9

Reference yield: 64.0%

Phenylselenyl bromide (34837-55-3) + phenylacetaldehyde (122-78-1) → (+/-)-2-phenylselenophenyacetaldehyde (82737-11-9)

Guidance literature:

With diisopropylamine; In tetrahydrofuran; for 1h; Ambient temperature;

DOI:10.1021/jo981693t

upstream raw materials:

1-(2-methoxyvinyl)benzene

Benzeneselenol

Phenylselenyl bromide

phenylacetaldehyde

Downstream raw materials:

1-[(2S,4aS,7R,8aR)-4,4,7-Trimethyl-2-(phenyl-phenylselanyl-methyl)-hexahydro-benzo[e][1,3]oxazin-3-yl]-propenone

(2S,3S,3aS,4aR,6R,8aS)-2,6,9,9-Tetramethyl-3-phenyl-octahydro-benzo[e]pyrrolo[2,1-b][1,3]oxazin-1-one

(2R,3S,3aS,4aR,6R,8aS)-2,6,9,9-Tetramethyl-3-phenyl-octahydro-benzo[e]pyrrolo[2,1-b][1,3]oxazin-1-one

(3'S,4'S)-8-(3'-methyl-4'-phenylpyrrolidinyl)-menthol

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