(3S,4R)-4-((S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoic acid

Base Information

Chemical Name:(3S,4R)-4-((S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoic acid
CAS No.:1146434-31-2
Molecular Formula:C₅₃H₆₄N₂O₆SSi
Molecular Weight:885.252
Hs Code.:

Synonyms:(3S,4R)-4-((S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoic acid

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Chemical Property of (3S,4R)-4-((S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoic acid

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Technology Process of (3S,4R)-4-((S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoic acid

There total 1 articles about (3S,4R)-4-((S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 663919-01-5
4R-[2-(9H-fluoren-9-ylmethoxycarbonylamino)-3S-tritylsulfanylpropionylamino]-5-methyl-3-triisopropylsilanyloxyhexanoic acid 2,2,2-trichloroethyl ester

: 1146434-31-2
(3S,4R)-4-((S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoic acid

Guidance literature:: With ammonium acetate; water; zinc; In tetrahydrofuran; at 20 ℃; for 19h; Inert atmosphere;
DOI:10.1021/ol900436f

Reference yield: 66.0%

: 1146434-43-6
(R)-((4R,5R)-5-(2-(2-methoxyethylamino)-2-oxoethoxy)-1,2-dithian-4-yl) 2-((S,E)-3-hydroxy-7-(tritylthio)hept-4-enamido)propanoate

: 1146434-31-2
(3S,4R)-4-((S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoic acid

: 1146434-44-7
(3S,4R)-((S,E)-1-((R)-1-((4R,5R)-5-(2-(2-methoxyethylamino)-2-oxoethoxy)-1,2-dithian-4-yloxy)-1-oxopropan-2-ylamino)-1-oxo-7-(tritylthio)hept-4-en-3-yl) 4-((S)-2-(((9H-fluoren-9-yl)-methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoate

Guidance literature:: (3S,4R)-4-((S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoic acid; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; for 0.333333h; Inert atmosphere;

(R)-((4R,5R)-5-(2-(2-methoxyethylamino)-2-oxoethoxy)-1,2-dithian-4-yl) 2-((S,E)-3-hydroxy-7-(tritylthio)hept-4-enamido)propanoate; With dmap; In tetrahydrofuran; at 20 ℃; for 15.5h; Inert atmosphere;
DOI:10.1021/ol900436f