(3S,4R)-((S,E)-1-((R)-1-((4R,5R)-5-(2-(2-methoxyethylamino)-2-oxoethoxy)-1,2-dithian-4-yloxy)-1-oxopropan-2-ylamino)-1-oxo-7-(tritylthio)hept-4-en-3-yl) 4-((S)-2-(((9H-fluoren-9-yl)-methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoate

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Chemical Name:(3S,4R)-((S,E)-1-((R)-1-((4R,5R)-5-(2-(2-methoxyethylamino)-2-oxoethoxy)-1,2-dithian-4-yloxy)-1-oxopropan-2-ylamino)-1-oxo-7-(tritylthio)hept-4-en-3-yl) 4-((S)-2-(((9H-fluoren-9-yl)-methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoate
CAS No.:1146434-44-7
Molecular Formula:C₉₁H₁₀₈N₄O₁₂S₄Si
Molecular Weight:1606.23
Hs Code.:

(3S,4R)-((S,E)-1-((R)-1-((4R,5R)-5-(2-(2-methoxyethylamino)-2-oxoethoxy)-1,2-dithian-4-yloxy)-1-oxopropan-2-ylamino)-1-oxo-7-(tritylthio)hept-4-en-3-yl) 4-((S)-2-(((9H-fluoren-9-yl)-methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoate

Synonyms:(3S,4R)-((S,E)-1-((R)-1-((4R,5R)-5-(2-(2-methoxyethylamino)-2-oxoethoxy)-1,2-dithian-4-yloxy)-1-oxopropan-2-ylamino)-1-oxo-7-(tritylthio)hept-4-en-3-yl) 4-((S)-2-(((9H-fluoren-9-yl)-methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoate

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Chemical Property of (3S,4R)-((S,E)-1-((R)-1-((4R,5R)-5-(2-(2-methoxyethylamino)-2-oxoethoxy)-1,2-dithian-4-yloxy)-1-oxopropan-2-ylamino)-1-oxo-7-(tritylthio)hept-4-en-3-yl) 4-((S)-2-(((9H-fluoren-9-yl)-methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoate

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Technology Process of (3S,4R)-((S,E)-1-((R)-1-((4R,5R)-5-(2-(2-methoxyethylamino)-2-oxoethoxy)-1,2-dithian-4-yloxy)-1-oxopropan-2-ylamino)-1-oxo-7-(tritylthio)hept-4-en-3-yl) 4-((S)-2-(((9H-fluoren-9-yl)-methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoate

There total 1 articles about (3S,4R)-((S,E)-1-((R)-1-((4R,5R)-5-(2-(2-methoxyethylamino)-2-oxoethoxy)-1,2-dithian-4-yloxy)-1-oxopropan-2-ylamino)-1-oxo-7-(tritylthio)hept-4-en-3-yl) 4-((S)-2-(((9H-fluoren-9-yl)-methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1146434-43-6
(R)-((4R,5R)-5-(2-(2-methoxyethylamino)-2-oxoethoxy)-1,2-dithian-4-yl) 2-((S,E)-3-hydroxy-7-(tritylthio)hept-4-enamido)propanoate

: 1146434-31-2
(3S,4R)-4-((S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoic acid

: 1146434-44-7
(3S,4R)-((S,E)-1-((R)-1-((4R,5R)-5-(2-(2-methoxyethylamino)-2-oxoethoxy)-1,2-dithian-4-yloxy)-1-oxopropan-2-ylamino)-1-oxo-7-(tritylthio)hept-4-en-3-yl) 4-((S)-2-(((9H-fluoren-9-yl)-methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoate

Guidance literature:: (3S,4R)-4-((S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylthio)propanamido)-5-methyl-3-(triisopropylsilyloxy)hexanoic acid; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; for 0.333333h; Inert atmosphere;

(R)-((4R,5R)-5-(2-(2-methoxyethylamino)-2-oxoethoxy)-1,2-dithian-4-yl) 2-((S,E)-3-hydroxy-7-(tritylthio)hept-4-enamido)propanoate; With dmap; In tetrahydrofuran; at 20 ℃; for 15.5h; Inert atmosphere;
DOI:10.1021/ol900436f