1-(2,3-difluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

Base Information

Chemical Name:1-(2,3-difluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide
CAS No.:1446712-62-4
Molecular Formula:C₁₄H₁₃F₂N₇
Molecular Weight:317.301
Hs Code.:

Synonyms:1-(2,3-difluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

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Chemical Property of 1-(2,3-difluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

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Technology Process of 1-(2,3-difluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

There total 6 articles about 1-(2,3-difluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1446712-60-2
1-(2,3-difluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidamide

: 1446712-62-4
1-(2,3-difluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

Guidance literature:: With hydrazine hydrate; triethylamine; In ethanol; at 0 - 20 ℃; for 72h; Inert atmosphere;

Reference yield:

: 1446712-58-8
1-(2,3-difluorobenzyl)-3-iodo-6-methyl-1H-pyrazolo[3,4-d]pyrimidine

: 1446712-62-4
1-(2,3-difluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: dimethyl sulfoxide / 2 h / 150 °C

2.1: sodium methylate / methanol / 1 h / 20 °C / Inert atmosphere

2.2: 2 h / Inert atmosphere; Reflux

3.1: triethylamine; hydrazine hydrate / ethanol / 72 h / 0 - 20 °C / Inert atmosphere

With sodium methylate; hydrazine hydrate; triethylamine; In methanol; ethanol; dimethyl sulfoxide;

Reference yield:

: 1446712-59-9
1-(2,3-difluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carbonitrile

: 1446712-62-4
1-(2,3-difluorobenzyl)-6-methyl-1H-pyrazolo[3,4-d]pyrimidine-3-carboximidohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 1 h / 20 °C / Inert atmosphere

1.2: 2 h / Inert atmosphere; Reflux

2.1: triethylamine; hydrazine hydrate / ethanol / 72 h / 0 - 20 °C / Inert atmosphere

With sodium methylate; hydrazine hydrate; triethylamine; In methanol; ethanol;