C₂₁H₁₇BrClF₆N₃O₃S

Base Information

Chemical Name:C₂₁H₁₇BrClF₆N₃O₃S
CAS No.:1450621-12-1
Molecular Formula:C₂₁H₁₇BrClF₆N₃O₃S
Molecular Weight:620.798
Hs Code.:

C<sub>21</sub>H<sub>17</sub>BrClF<sub>6</sub>N<sub>3</sub>O<sub>3</sub>S

Synonyms:C₂₁H₁₇BrClF₆N₃O₃S

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Chemical Property of C₂₁H₁₇BrClF₆N₃O₃S

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Technology Process of C₂₁H₁₇BrClF₆N₃O₃S

There total 12 articles about C₂₁H₁₇BrClF₆N₃O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1450620-14-0
4-benzyl 1-tert-butyl 2-(1-propyn-1-yl)-1,4-piperazinedicarboxylate

: 1450621-12-1
C₂₁H₁₇BrClF₆N₃O₃S

Guidance literature:: Multi-step reaction with 5 steps

1: Chiralpak^? ADH column / ethanol / Resolution of racemate

2: trifluoroacetic acid / dichloromethane / 0.67 h / 20 °C

3: ruphos; chloro-(2-dicyclohexylphosphino-2’,6’-diisopropoxy-1,1‘-biphenyl)[2-(2-aminoethyl)phenyl] palladium(ll) methyl-tert-butyl ether adduct / toluene / 2.33 h / 100 °C / Inert atmosphere

4: trifluorormethanesulfonic acid; trifluoroacetic acid / 0.17 h

5: triethylamine / dichloromethane / 0.22 h / 0 °C

With trifluorormethanesulfonic acid; chloro-(2-dicyclohexylphosphino-2’,6’-diisopropoxy-1,1‘-biphenyl)[2-(2-aminoethyl)phenyl] palladium(ll) methyl-tert-butyl ether adduct; triethylamine; trifluoroacetic acid; ruphos; In ethanol; dichloromethane; toluene;

Reference yield:

: 1450621-77-8
ethyl 2-[benzyl-[(2S)-2-(tert-butoxycarbonylamino)pent-4-ynoyl]amino]acetate

: 1450621-12-1
C₂₁H₁₇BrClF₆N₃O₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

1.2: 0.17 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 65 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 20 °C

4.1: ruphos; chloro-(2-dicyclohexylphosphino-2’,6’-diisopropoxy-1,1‘-biphenyl)[2-(2-aminoethyl)phenyl] palladium(ll) methyl-tert-butyl ether adduct; sodium t-butanolate / 1,4-dioxane / 12 h / 80 °C

5.1: carbonochloridic acid 1-chloro-ethyl ester; potassium carbonate / dichloromethane / 0.5 h / 20 °C

6.1: triethylamine / dichloromethane / 0.22 h / 0 °C

With lithium aluminium tetrahydride; carbonochloridic acid 1-chloro-ethyl ester; chloro-(2-dicyclohexylphosphino-2’,6’-diisopropoxy-1,1‘-biphenyl)[2-(2-aminoethyl)phenyl] palladium(ll) methyl-tert-butyl ether adduct; potassium tert-butylate; potassium carbonate; triethylamine; trifluoroacetic acid; sodium t-butanolate; ruphos; In tetrahydrofuran; 1,4-dioxane; dichloromethane;

Reference yield:

: 1450621-79-0
(3S)-1-benzyl-3-(2-propyn-1-yl)-piperazine

: 1450621-12-1
C₂₁H₁₇BrClF₆N₃O₃S

Guidance literature:: Multi-step reaction with 4 steps

1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 20 °C

2: ruphos; chloro-(2-dicyclohexylphosphino-2’,6’-diisopropoxy-1,1‘-biphenyl)[2-(2-aminoethyl)phenyl] palladium(ll) methyl-tert-butyl ether adduct; sodium t-butanolate / 1,4-dioxane / 12 h / 80 °C

3: carbonochloridic acid 1-chloro-ethyl ester; potassium carbonate / dichloromethane / 0.5 h / 20 °C

4: triethylamine / dichloromethane / 0.22 h / 0 °C

With carbonochloridic acid 1-chloro-ethyl ester; chloro-(2-dicyclohexylphosphino-2’,6’-diisopropoxy-1,1‘-biphenyl)[2-(2-aminoethyl)phenyl] palladium(ll) methyl-tert-butyl ether adduct; potassium tert-butylate; potassium carbonate; triethylamine; sodium t-butanolate; ruphos; In tetrahydrofuran; 1,4-dioxane; dichloromethane;