2-(2-formyl-4,5-dimethoxyphenylethyl)-6,7-dimethoxyphthalimidine

Base Information

Chemical Name:2-(2-formyl-4,5-dimethoxyphenylethyl)-6,7-dimethoxyphthalimidine
CAS No.:710336-24-6
Molecular Formula:C₂₁H₂₃NO₆
Molecular Weight:385.417
Hs Code.:

Synonyms:2-(2-formyl-4,5-dimethoxyphenylethyl)-6,7-dimethoxyphthalimidine

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Chemical Property of 2-(2-formyl-4,5-dimethoxyphenylethyl)-6,7-dimethoxyphthalimidine

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Technology Process of 2-(2-formyl-4,5-dimethoxyphenylethyl)-6,7-dimethoxyphthalimidine

There total 3 articles about 2-(2-formyl-4,5-dimethoxyphenylethyl)-6,7-dimethoxyphthalimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 3344-74-9
2-(3,4-dimethoxyphenethyl)-6,7-dimethoxyisoindolin-1-one

: 4885-02-3
Dichloromethyl methyl ether

: 710336-24-6
2-(2-formyl-4,5-dimethoxyphenylethyl)-6,7-dimethoxyphthalimidine

Guidance literature:: With titanium tetrachloride; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/j.tet.2004.03.049

Reference yield:

: 65495-31-0
6-(chloromethyl)-2,3-dimethoxybenzoic acid ethyl ester

: 710336-24-6
2-(2-formyl-4,5-dimethoxyphenylethyl)-6,7-dimethoxyphthalimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / triethylamine / acetonitrile / 3 h / Heating

2: 96 percent / TiCl₄ / CH₂Cl₂ / 3 h / 20 °C

With titanium tetrachloride; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2004.03.049

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 710336-24-6
2-(2-formyl-4,5-dimethoxyphenylethyl)-6,7-dimethoxyphthalimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / triethylamine / acetonitrile / 3 h / Heating

2: 96 percent / TiCl₄ / CH₂Cl₂ / 3 h / 20 °C

With titanium tetrachloride; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2004.03.049