methyl 2-benzyl-3-(methoxycarbonyl)-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionate

Base Information

• Chemical Name: methyl 2-benzyl-3-(methoxycarbonyl)-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionate
• CAS No.: 19171-89-2
• Molecular Formula: C₂₅H₂₈N₂O₄
• Molecular Weight: 420.508

Synonyms:methyl 2-benzyl-3-(methoxycarbonyl)-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionate

Chemical Property of methyl 2-benzyl-3-(methoxycarbonyl)-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionate

Chemical Property:

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Technology Process of methyl 2-benzyl-3-(methoxycarbonyl)-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionate

There total 17 articles about methyl 2-benzyl-3-(methoxycarbonyl)-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.7%

diazomethane (186581-53-3,908094-01-9,334-88-3) + trans-2-benzyl-3-methoxycarbonyl-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionic acid (60702-96-7,91219-81-7,91219-82-8) → methyl trans-2-benzyl-3-methoxycarbonyl-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionate (4837-57-4,19171-89-2,47679-01-6,84129-60-2,91279-02-6,120056-44-2,141847-51-0,142292-54-4)

Guidance literature:

In methanol; dichloromethane; for 1h; Ambient temperature;

Reference yield: 91.0%

methanol (67-56-1) + 2-benzyl-3-(methoxycarbonyl)-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionic acid (60702-96-7) → methyl 2-benzyl-3-(methoxycarbonyl)-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionate (19171-89-2)

Guidance literature:

With hydrogenchloride; for 2.5h; Heating;

DOI:10.1021/ja00342a045

Reference yield: 91.0%

methanol (67-56-1) + 2-benzyl-3-(methoxycarbonyl)-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionic acid (60702-96-7) → methyl trans-2-benzyl-3-methoxycarbonyl-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionate (4837-57-4,19171-89-2,47679-01-6,84129-60-2,91279-02-6,120056-44-2,141847-51-0,142292-54-4)

Guidance literature:

With hydrogenchloride; for 3h; Heating;

DOI:10.1016/S0040-4020(01)88507-0

upstream raw materials:

methanol

2-benzyl-3-(methoxycarbonyl)-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionic acid

benzaldehyde

N_a-methyl tryptophan methyl ester

Downstream raw materials:

methyl 5-methyl-9-oxo-12-benzyl-6,7,8,9,10,11-hexahydro-6,10-imino-5H-cyclooctaindole-8-carboxylate

methyl trans-2-benzyl-3-methoxycarbonyl-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionate

(-)-2-benzyl-3-carboxy-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionic acid

trans-2-benzyl-3-carboxy-9-methyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole-1-propionic acid

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