C₃₂H₃₃NO₄S

Base Information

Chemical Name:C₃₂H₃₃NO₄S
CAS No.:1424888-19-6
Molecular Formula:C₃₂H₃₃NO₄S
Molecular Weight:527.684
Hs Code.:

C<sub>32</sub>H<sub>33</sub>NO<sub>4</sub>S

Synonyms:C₃₂H₃₃NO₄S

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Chemical Property of C₃₂H₃₃NO₄S

Chemical Property:

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Technology Process of C₃₂H₃₃NO₄S

There total 9 articles about C₃₂H₃₃NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1424888-17-4
C₂₅H₂₇NO₄S

: 100-39-0
benzyl bromide

: 1424888-19-6
C₃₂H₃₃NO₄S

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2013.01.034

Reference yield:

: 1424888-75-4
C₂₅H₃₈N₂O₅SSi

: 1424888-19-6
C₃₂H₃₃NO₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / dichloromethane; hexane / -78 °C

1.2: -78 °C

2.1: dichloromethane / 12 h / 20 °C

3.1: diisobutylaluminium hydride / dichloromethane; hexane / -78 °C

3.2: -78 °C

4.1: manganese(IV) oxide / dichloromethane / 6 h / 20 °C

5.1: magnesium / tetrahydrofuran / 2 h / 20 °C

5.2: 0.08 h / 0 °C

6.1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

With manganese(IV) oxide; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; potassium carbonate; magnesium; acetic acid; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2013.01.034

Reference yield:

: C₂₃H₃₃NO₄SSi

: 1424888-19-6
C₃₂H₃₃NO₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: dichloromethane / 12 h / 20 °C

2.1: diisobutylaluminium hydride / dichloromethane; hexane / -78 °C

2.2: -78 °C

3.1: manganese(IV) oxide / dichloromethane / 6 h / 20 °C

4.1: magnesium / tetrahydrofuran / 2 h / 20 °C

4.2: 0.08 h / 0 °C

5.1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C

6.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

With manganese(IV) oxide; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; potassium carbonate; magnesium; acetic acid; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2013.01.034