S-[2-(N-benzyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

Base Information

Chemical Name:S-[2-(N-benzyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate
CAS No.:352556-36-6
Molecular Formula:C₂₆H₂₆N₂OS
Molecular Weight:414.571
Hs Code.:

Synonyms:S-[2-(N-benzyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

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Chemical Property of S-[2-(N-benzyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

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Technology Process of S-[2-(N-benzyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

There total 5 articles about S-[2-(N-benzyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 100-39-0
benzyl bromide

: 352556-29-7
S-[2-(N-3'-p-tolylprop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

: 352556-36-6
S-[2-(N-benzyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

Guidance literature:: With potassium carbonate; In acetone; for 15h; Heating;
DOI:10.1021/jo001783+

Reference yield:

: 624-31-7
4-tolyl iodide

: 352556-36-6
S-[2-(N-benzyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CuI; Et₃N / PdCl₂(PPh₃)2 / acetonitrile / 24 h / 20 °C

2: 88 percent / K₂CO₃ / acetone / 15 h / Heating

With copper(l) iodide; potassium carbonate; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In acetone; acetonitrile;
DOI:10.1021/jo001783+

Reference yield:

: 13511-84-7
S-(2-nitrophenyl)-N,N-dimethylcarbamothioate

: 352556-36-6
S-[2-(N-benzyl-N-3'-p-tolyl-prop-2'-ynyl)aminophenyl]-N,N-dimethylthiocarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 89 percent / Fe; water; glacial acetic acid / 8 h / 20 °C

2.1: K₂CO₃ / acetone / 5 h / 20 °C

2.2: 84 percent / acetone / 16 h / Heating

3.1: 92 percent / CuI; Et₃N / PdCl₂(PPh₃)2 / acetonitrile / 24 h / 20 °C

4.1: 88 percent / K₂CO₃ / acetone / 15 h / Heating

With copper(l) iodide; water; iron; potassium carbonate; acetic acid; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In acetone; acetonitrile;
DOI:10.1021/jo001783+