N-(2-chloroacetyl)-4-chloro-α-hydroxy-α,α-diphenyl-o-toluidyne

Base Information

Chemical Name:N-(2-chloroacetyl)-4-chloro-α-hydroxy-α,α-diphenyl-o-toluidyne
CAS No.:98414-59-6
Molecular Formula:C₂₁H₁₇Cl₂NO₂
Molecular Weight:386.277
Hs Code.:

Synonyms:N-(2-chloroacetyl)-4-chloro-α-hydroxy-α,α-diphenyl-o-toluidyne

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Chemical Property of N-(2-chloroacetyl)-4-chloro-α-hydroxy-α,α-diphenyl-o-toluidyne

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Technology Process of N-(2-chloroacetyl)-4-chloro-α-hydroxy-α,α-diphenyl-o-toluidyne

There total 1 articles about N-(2-chloroacetyl)-4-chloro-α-hydroxy-α,α-diphenyl-o-toluidyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 21741-00-4
(2-amino-5-chlorophenyl)diphenylmethanol

: 79-04-9
chloroacetyl chloride

: 98414-59-6
N-(2-chloroacetyl)-4-chloro-α-hydroxy-α,α-diphenyl-o-toluidyne

Guidance literature:: With triethylamine; In diethyl ether; 1.) 5 deg C, 1 h, 2.) RT, 18 h;
DOI:10.1021/jo00375a046

Reference yield: 74.0%

: 98414-59-6
N-(2-chloroacetyl)-4-chloro-α-hydroxy-α,α-diphenyl-o-toluidyne

: 98414-60-9
7-chloro-1,5-dihydro-5,5-diphenyl-4,1-benzoxazepin-2-(3H)-one

Guidance literature:: With sodium hydride; In tetrahydrofuran; 1.) RT, 20 h, 2.) reflux, 1.75 h;
DOI:10.1021/jo00375a046

Reference yield:

: 98414-59-6
N-(2-chloroacetyl)-4-chloro-α-hydroxy-α,α-diphenyl-o-toluidyne

: 105104-38-9
5-chloro-1-methyl-3,3-diphenyl-2-indolinecarboxaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / NaH / tetrahydrofuran / 1.) RT, 20 h, 2.) reflux, 1.75 h

2: 1.) sodium hydride / 1.) DMF, 2.25 h, 2.) DMF, 24 h

3: 1.5 g / LAH / tetrahydrofuran / 19.5 h / Ambient temperature

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo00375a046