methyl 2-(3-butenyl)-3-benzoylpropionate

Base Information

Chemical Name:methyl 2-(3-butenyl)-3-benzoylpropionate
CAS No.:172980-67-5
Molecular Formula:C₁₅H₁₈O₃
Molecular Weight:246.306
Hs Code.:

Synonyms:methyl 2-(3-butenyl)-3-benzoylpropionate

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Chemical Property of methyl 2-(3-butenyl)-3-benzoylpropionate

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Technology Process of methyl 2-(3-butenyl)-3-benzoylpropionate

There total 3 articles about methyl 2-(3-butenyl)-3-benzoylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 172980-66-4
methyl 2-(3-butenyl)-3-benzoylpropionate ethylene ketal

: 172980-67-5
methyl 2-(3-butenyl)-3-benzoylpropionate

Guidance literature:: With pyridinium p-toluenesulfonate; In diethyl ether; acetone; at 80 ℃; for 12h;
DOI:10.1021/jo951576n

Reference yield:

: 25333-24-8
3-benzoylpropionic acid methyl ester

: 172980-67-5
methyl 2-(3-butenyl)-3-benzoylpropionate

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / p-TsOH / benzene / Heating

2: 1.) LDA / 1.) THF, 25 deg C, 5 h, 2.) reflux, 24 h

3: 89 percent / pyridinium p-toluenesulfonate / acetone; diethyl ether / 12 h / 80 °C

With pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; lithium diisopropyl amide; In diethyl ether; acetone; benzene;
DOI:10.1021/jo951576n

Reference yield:

: 103632-91-3
2-[2-(methoxycarbonyl)ethyl]-2-phenyl-1,3-dioxolane

: 172980-67-5
methyl 2-(3-butenyl)-3-benzoylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA / 1.) THF, 25 deg C, 5 h, 2.) reflux, 24 h

2: 89 percent / pyridinium p-toluenesulfonate / acetone; diethyl ether / 12 h / 80 °C

With pyridinium p-toluenesulfonate; lithium diisopropyl amide; In diethyl ether; acetone;
DOI:10.1021/jo951576n