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Technology Process of F2B(C4N(CH3)(C2H5)CHCHC6H4OCH3)CC6H4O(CH2)6N3(C4N(CH3)C2H5CHCHC6H4NCH2CH2SCH2CH2OCH2CH2OCH2CH2SCH2CH2)

F2B(C4N(CH3)(C2H5)CHCHC6H4OCH3)CC6H4O(CH2)6N3(C4N(CH3)C2H5CHCHC6H4NCH2CH2SCH2CH2OCH2CH2OCH2CH2SCH2CH2)

Base Information
  • Chemical Name:F2B(C4N(CH3)(C2H5)CHCHC6H4OCH3)CC6H4O(CH2)6N3(C4N(CH3)C2H5CHCHC6H4NCH2CH2SCH2CH2OCH2CH2OCH2CH2SCH2CH2)
  • CAS No.:1351657-24-3
  • Molecular Formula:C54H67BF2N6O4S2
  • Molecular Weight:977.104
  • Hs Code.:
F<sub>2</sub>B(C<sub>4</sub>N(CH<sub>3</sub>)(C<sub>2</sub>H<sub>5</sub>)CHCHC<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)CC<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)6N<sub>3</sub>(C<sub>4</sub>N(CH<sub>3</sub>)C<sub>2</sub>H<sub>5</sub>CHCHC<sub>6</sub>H<sub>4</sub>NCH<sub>2</sub>CH<sub>2</sub>SCH<sub>2</sub>CH<sub>2</sub>OCH<sub>2</sub>CH<sub>2</sub>OCH<sub>2</sub>CH<sub>2</sub>SCH<sub>2</sub>CH<sub>2</sub>)

Synonyms:F2B(C4N(CH3)(C2H5)CHCHC6H4OCH3)CC6H4O(CH2)6N3(C4N(CH3)C2H5CHCHC6H4NCH2CH2SCH2CH2OCH2CH2OCH2CH2SCH2CH2)

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Chemical Property of F2B(C4N(CH3)(C2H5)CHCHC6H4OCH3)CC6H4O(CH2)6N3(C4N(CH3)C2H5CHCHC6H4NCH2CH2SCH2CH2OCH2CH2OCH2CH2SCH2CH2)
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Technology Process of F2B(C4N(CH3)(C2H5)CHCHC6H4OCH3)CC6H4O(CH2)6N3(C4N(CH3)C2H5CHCHC6H4NCH2CH2SCH2CH2OCH2CH2OCH2CH2SCH2CH2)

There total 6 articles about F2B(C4N(CH3)(C2H5)CHCHC6H4OCH3)CC6H4O(CH2)6N3(C4N(CH3)C2H5CHCHC6H4NCH2CH2SCH2CH2OCH2CH2OCH2CH2SCH2CH2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

F<sub>2</sub>B(C<sub>4</sub>N(CH<sub>3</sub>)2C<sub>2</sub>H<sub>5</sub>)CC<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)6N<sub>3</sub>(C<sub>4</sub>N(CH<sub>3</sub>)C<sub>2</sub>H<sub>5</sub>CHCHC<sub>6</sub>H<sub>4</sub>NCH<sub>2</sub>CH<sub>2</sub>SCH<sub>2</sub>CH<sub>2</sub>OCH<sub>2</sub>CH<sub>2</sub>OCH<sub>2</sub>CH<sub>2</sub>SCH<sub>2</sub>CH<sub>2</sub>)
1351657-23-2

F2B(C4N(CH3)2C2H5)CC6H4O(CH2)6N3(C4N(CH3)C2H5CHCHC6H4NCH2CH2SCH2CH2OCH2CH2OCH2CH2SCH2CH2)

4-methoxy-benzaldehyde
123-11-5

4-methoxy-benzaldehyde

F<sub>2</sub>B(C<sub>4</sub>N(CH<sub>3</sub>)(C<sub>2</sub>H<sub>5</sub>)CHCHC<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)CC<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)6N<sub>3</sub>(C<sub>4</sub>N(CH<sub>3</sub>)C<sub>2</sub>H<sub>5</sub>CHCHC<sub>6</sub>H<sub>4</sub>NCH<sub>2</sub>CH<sub>2</sub>SCH<sub>2</sub>CH<sub>2</sub>OCH<sub>2</sub>CH<sub>2</sub>OCH<sub>2</sub>CH<sub>2</sub>SCH<sub>2</sub>CH<sub>2</sub>)
1351657-24-3

F2B(C4N(CH3)(C2H5)CHCHC6H4OCH3)CC6H4O(CH2)6N3(C4N(CH3)C2H5CHCHC6H4NCH2CH2SCH2CH2OCH2CH2OCH2CH2SCH2CH2)

Guidance literature:
With piperidine; acetic acid; In benzene; for 2h; Reflux;
DOI:10.1002/anie.201104228

Reference yield:

2,4-dimethyl-3-ethyl-pyrrole
517-22-6

2,4-dimethyl-3-ethyl-pyrrole

F<sub>2</sub>B(C<sub>4</sub>N(CH<sub>3</sub>)(C<sub>2</sub>H<sub>5</sub>)CHCHC<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)CC<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)6N<sub>3</sub>(C<sub>4</sub>N(CH<sub>3</sub>)C<sub>2</sub>H<sub>5</sub>CHCHC<sub>6</sub>H<sub>4</sub>NCH<sub>2</sub>CH<sub>2</sub>SCH<sub>2</sub>CH<sub>2</sub>OCH<sub>2</sub>CH<sub>2</sub>OCH<sub>2</sub>CH<sub>2</sub>SCH<sub>2</sub>CH<sub>2</sub>)
1351657-24-3

F2B(C4N(CH3)(C2H5)CHCHC6H4OCH3)CC6H4O(CH2)6N3(C4N(CH3)C2H5CHCHC6H4NCH2CH2SCH2CH2OCH2CH2OCH2CH2SCH2CH2)

Guidance literature:
Multi-step reaction with 5 steps
1.1: trifluoroacetic acid / dichloromethane / 12 h / 20 °C / Inert atmosphere
1.2: 0.75 h / 20 °C / Inert atmosphere
2.1: boron trifluoride diethyl etherate; triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
3.1: sodium azide / dimethyl sulfoxide / 0.5 h / 60 °C
4.1: piperidine; acetic acid / benzene / 2 h / Reflux
5.1: piperidine; acetic acid / benzene / 2 h / Reflux
With piperidine; sodium azide; boron trifluoride diethyl etherate; acetic acid; triethylamine; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide; benzene;
DOI:10.1002/anie.201104228

Reference yield:

F<sub>2</sub>B(C<sub>4</sub>N(CH<sub>3</sub>)2C<sub>2</sub>H<sub>5</sub>)2CC<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)6Br
1351657-21-0

F2B(C4N(CH3)2C2H5)2CC6H4O(CH2)6Br

F<sub>2</sub>B(C<sub>4</sub>N(CH<sub>3</sub>)(C<sub>2</sub>H<sub>5</sub>)CHCHC<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)CC<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)6N<sub>3</sub>(C<sub>4</sub>N(CH<sub>3</sub>)C<sub>2</sub>H<sub>5</sub>CHCHC<sub>6</sub>H<sub>4</sub>NCH<sub>2</sub>CH<sub>2</sub>SCH<sub>2</sub>CH<sub>2</sub>OCH<sub>2</sub>CH<sub>2</sub>OCH<sub>2</sub>CH<sub>2</sub>SCH<sub>2</sub>CH<sub>2</sub>)
1351657-24-3

F2B(C4N(CH3)(C2H5)CHCHC6H4OCH3)CC6H4O(CH2)6N3(C4N(CH3)C2H5CHCHC6H4NCH2CH2SCH2CH2OCH2CH2OCH2CH2SCH2CH2)

Guidance literature:
Multi-step reaction with 3 steps
1: sodium azide / dimethyl sulfoxide / 0.5 h / 60 °C
2: piperidine; acetic acid / benzene / 2 h / Reflux
3: piperidine; acetic acid / benzene / 2 h / Reflux
With piperidine; sodium azide; acetic acid; In dimethyl sulfoxide; benzene;
DOI:10.1002/anie.201104228
upstream raw materials:

2,4-dimethyl-3-ethyl-pyrrole

F2B(C4N(CH3)2C2H5)2CC6H4O(CH2)6Br

F2B(C4N(CH3)2C2H5)CC6H4O(CH2)6N3(C4N(CH3)C2H5CHCHC6H4NCH2CH2SCH2CH2OCH2CH2OCH2CH2SCH2CH2)

4-methoxy-benzaldehyde

Downstream raw materials:

F2B(C4NH(CH3)2)C4NHCH3C2H2C6H4OCH2CCHN3C6H12OC6H4CBF2(C4NCH3C2H5)2CHCHC6H4OCH3(CHCHC6H4N(C4H8SO)2C2H4)CC6H4N(CH2C5H4N)2

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