Tris(trimethylsilyl)iodsilan

Base Information

• Chemical Name: Tris(trimethylsilyl)iodsilan
• CAS No.: 26245-35-2
• Molecular Formula: C₉H₂₇ISi₄
• Molecular Weight: 374.56
• Mol file: 26245-35-2.mol

Synonyms:Tris(trimethylsilyl)iodsilan

Chemical Property of Tris(trimethylsilyl)iodsilan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of Tris(trimethylsilyl)iodsilan

There total 1 articles about Tris(trimethylsilyl)iodsilan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

[ZnI(Si(SiMe3)3)(THF)]2 → Tris(trimethylsilyl)iodsilan (26245-35-2) + zinc (7440-66-6)

Guidance literature:

at 250 ℃; for 4h; Inert atmosphere;

DOI:10.1021/ic502184f

Reference yield:

Tris(trimethylsilyl)iodsilan (26245-35-2) → tris-(trimethylsilyl)silane (1873-77-4)

Guidance literature:

With sodium tetrahydroborate;

DOI:10.1016/S0040-4039(00)99111-1

Reference yield:

Tris(trimethylsilyl)iodsilan (26245-35-2) → C31H45BN2Si3

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 0.17 h / 20 °C

2: benzene / 0.17 h / 20 °C / Schlenk technique

In benzene;

DOI:10.1021/acs.organomet.1c00380

Downstream raw materials:

tris-(trimethylsilyl)silane

Refernces