N-(p-methoxyphenyl)pent-4-enaldimine

Base Information

Chemical Name:N-(p-methoxyphenyl)pent-4-enaldimine
CAS No.:286933-13-9
Molecular Formula:C₁₂H₁₅NO
Molecular Weight:189.257
Hs Code.:

Synonyms:N-(p-methoxyphenyl)pent-4-enaldimine

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Chemical Property of N-(p-methoxyphenyl)pent-4-enaldimine

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Technology Process of N-(p-methoxyphenyl)pent-4-enaldimine

There total 1 articles about N-(p-methoxyphenyl)pent-4-enaldimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2100-17-6
4-pentenal

: 104-94-9
4-methoxy-aniline

: 286933-13-9
N-(p-methoxyphenyl)pent-4-enaldimine

Guidance literature:: 4-pentenal; 4-methoxy-aniline; In diethyl ether; at 0 ℃; for 0.25h;

With potassium hydroxide; In diethyl ether; for 0.25h;

Reference yield: 56.0%

: 286933-13-9
N-(p-methoxyphenyl)pent-4-enaldimine

: 132127-27-6
(1R,2S)-2-phenyl-1-cyclohexyl<(triisopropylsilyl)oxy>acetate

: 286933-02-6
(3R,4S)-1-(4-methoxyphenyl)-3-triisopropylsiloxy-4-(3-butenyl)azetidin-2-one

Guidance literature:: (1R,2S)-2-phenyl-1-cyclohexyl<(triisopropylsilyl)oxy>acetate; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -84 ℃;

N-(p-methoxyphenyl)pent-4-enaldimine; In tetrahydrofuran; at -84 - 20 ℃; Further stages.;
DOI:10.1021/ja000293w

Reference yield: 55.0%

: 286933-13-9
N-(p-methoxyphenyl)pent-4-enaldimine

: 622-42-4
1-nitro-1-phenylmethane

: 407-25-0
trifluoroacetic anhydride

: 2,2,2-trifluoro-N-(4-methoxyphenyl)-N-((1S*,2R*)-1-nitro-1-phenylhex-5-en-2-yl)acetamide

Guidance literature:: 1-nitro-1-phenylmethane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; Inert atmosphere; Schlenk technique;

N-(p-methoxyphenyl)pent-4-enaldimine; With trifluoroacetic acid; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h; Inert atmosphere; Schlenk technique;

trifluoroacetic anhydride; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 - 25 ℃; for 18h; diastereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tet.2018.06.022