2,4-di-tert-butyl-6-{[(2'-hydroxyethyl)(methyl)amino]methyl}phenol

Base Information

• Chemical Name: 2,4-di-tert-butyl-6-{[(2'-hydroxyethyl)(methyl)amino]methyl}phenol
• CAS No.: 209681-64-1
• Molecular Formula: C₁₈H₃₁NO₂
• Molecular Weight: 293.45
• Mol file: 209681-64-1.mol

Synonyms:2,4-di-tert-butyl-6-{[(2'-hydroxyethyl)(methyl)amino]methyl}phenol

Chemical Property of 2,4-di-tert-butyl-6-{[(2'-hydroxyethyl)(methyl)amino]methyl}phenol

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2,4-di-tert-butyl-6-{[(2'-hydroxyethyl)(methyl)amino]methyl}phenol

There total 1 articles about 2,4-di-tert-butyl-6-{[(2'-hydroxyethyl)(methyl)amino]methyl}phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(2-hydroxyethyl)(methyl)amine (109-83-1) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2,4-di-tert-Butylphenol (96-76-4) → 2,4-di-tert-butyl-6-{[(2'-hydroxyethyl)(methyl)amino]methyl}phenol (209681-64-1)

Guidance literature:

at 120 ℃; Neat (no solvent);

DOI:10.1002/ejic.201001201

Reference yield: 90.0%

bis[N,N-bistrimethylsilylamido]bis(tetrahydrofuran)ytterbium(II) (154671-38-2) + 2,4-di-tert-butyl-6-{[(2'-hydroxyethyl)(methyl)amino]methyl}phenol (209681-64-1) → [Yb(2,4-di-tert-butyl-6-([(2'-hydroxyethyl)methylamino]methyl)phenol(2-))]2

Guidance literature:

In hexane; under N2 atm. soln. Yb complex in hexane was treated at room temp. with soln. ligand in hexane and stirred overnight; elem. anal.;

DOI:10.1039/b821770j

Reference yield: 74.0%

2,4-di-tert-butyl-6-{[(2'-hydroxyethyl)(methyl)amino]methyl}phenol (209681-64-1) → C18H29NO2(2-)*2Na(1+)

Guidance literature:

With sodium hexamethyldisilazane; In tetrahydrofuran; for 18h;

DOI:10.1080/00958972.2018.1445237

upstream raw materials:

(2-hydroxyethyl)(methyl)amine

formaldehyd

2,4-di-tert-Butylphenol