(4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)hydroxyacetic acid ethyl ester

Base Information

Chemical Name:(4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)hydroxyacetic acid ethyl ester
CAS No.:1186634-13-8
Molecular Formula:C₃₄H₃₆N₂O₅S
Molecular Weight:584.736
Hs Code.:

Synonyms:(4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)hydroxyacetic acid ethyl ester

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Chemical Property of (4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)hydroxyacetic acid ethyl ester

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Technology Process of (4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)hydroxyacetic acid ethyl ester

There total 9 articles about (4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)hydroxyacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.2%

: 1186634-26-3
4-(4-cyclohexylbenzyloxy)benzaldehyde

: 1186634-12-7
hydroxy(4-(3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)acetic acid ethyl ester

: 1186634-13-8
(4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)hydroxyacetic acid ethyl ester

Guidance literature:: With piperidine; In ethanol; for 16h; Reflux;

Reference yield:

: 121986-07-0,137766-69-9,13312-80-6
p-nitromandelonitrile

: 1186634-13-8
(4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)hydroxyacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride / water; acetic acid / 4 h / 100 °C

1.2: 4 h / 80 - 85 °C

2.1: hydrogen / palladium on activated charcoal / methanol / 4 h

3.1: ethanol / 6 h / Reflux

4.1: triethylamine / ethanol / 5 h / Reflux

5.1: piperidine / ethanol / 16 h / Reflux

With piperidine; hydrogenchloride; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; water; acetic acid;

Reference yield:

4-nitro-mandelic acid-ethyl ester: 13312-87-3
4-nitro-mandelic acid-ethyl ester

: 1186634-13-8
(4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)hydroxyacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / palladium on activated charcoal / methanol / 4 h

2: ethanol / 6 h / Reflux

3: triethylamine / ethanol / 5 h / Reflux

4: piperidine / ethanol / 16 h / Reflux

With piperidine; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol;