ethyl {4-[4-(adamant-1-yl)butyl]phenyl}acetate

Base Information

Chemical Name:ethyl {4-[4-(adamant-1-yl)butyl]phenyl}acetate
CAS No.:1305348-92-8
Molecular Formula:C₂₄H₃₄O₂
Molecular Weight:354.533
Hs Code.:

Synonyms:ethyl {4-[4-(adamant-1-yl)butyl]phenyl}acetate

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Chemical Property of ethyl {4-[4-(adamant-1-yl)butyl]phenyl}acetate

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Technology Process of ethyl {4-[4-(adamant-1-yl)butyl]phenyl}acetate

There total 15 articles about ethyl {4-[4-(adamant-1-yl)butyl]phenyl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 64-17-5
ethanol

: 1305348-93-9
C₂₂H₂₈N₂O

: 1305348-92-8
ethyl {4-[4-(adamant-1-yl)butyl]phenyl}acetate

Guidance literature:: With silver benzoate; triethylamine; at 90 ℃; for 0.75h;

Reference yield:

: 2094-74-8
1-Adamantanecarbaldehyde

: 1305348-92-8
ethyl {4-[4-(adamant-1-yl)butyl]phenyl}acetate

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C

1.2: 1 h / 0 - 5 °C

2.1: sodium hydroxide; water / methanol / 2 h / 70 °C

2.2: 0.5 h / 4 °C / pH 2

3.1: hydrogen / palladium 10% on activated carbon / methanol / 0.25 h / 2068.65 Torr

4.1: sulfuric acid / 3 h / 80 °C

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.25 h / 0 - 20 °C

6.1: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C

7.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C

7.2: 1 h / 0 - 5 °C

8.1: sodium hydroxide; water / methanol / 2 h / 70 °C

8.2: 0.5 h / 4 °C / pH 2

9.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 0.25 h

10.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 3 h / 50 °C

10.2: 3 h / 0 °C

11.1: triethylamine; silver benzoate / 0.75 h / 90 °C

With lithium aluminium tetrahydride; oxalyl dichloride; sulfuric acid; water; hydrogen; silver benzoate; sodium hydride; triethylamine; N,N-dimethyl-formamide; pyridinium chlorochromate; sodium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 711-01-3
methyl adamantane-1-carboxylate

: 1305348-92-8
ethyl {4-[4-(adamant-1-yl)butyl]phenyl}acetate

Guidance literature:: Multi-step reaction with 13 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.25 h / 0 - 20 °C

2.1: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C

3.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C

3.2: 1 h / 0 - 5 °C

4.1: sodium hydroxide; water / methanol / 2 h / 70 °C

4.2: 0.5 h / 4 °C / pH 2

5.1: hydrogen / palladium 10% on activated carbon / methanol / 0.25 h / 2068.65 Torr

6.1: sulfuric acid / 3 h / 80 °C

7.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.25 h / 0 - 20 °C

8.1: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C

9.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C

9.2: 1 h / 0 - 5 °C

10.1: sodium hydroxide; water / methanol / 2 h / 70 °C

10.2: 0.5 h / 4 °C / pH 2

11.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 0.25 h

12.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 3 h / 50 °C

12.2: 3 h / 0 °C

13.1: triethylamine; silver benzoate / 0.75 h / 90 °C

With lithium aluminium tetrahydride; oxalyl dichloride; sulfuric acid; water; hydrogen; silver benzoate; sodium hydride; triethylamine; N,N-dimethyl-formamide; pyridinium chlorochromate; sodium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane;