(1RS,2SR)-5,5-ethylenedioxy-2-(N-methylamidomethyl)-2-(3',4'-dimethoxyphenyl)cyclohexyl acetate

Base Information

Chemical Name:(1RS,2SR)-5,5-ethylenedioxy-2-(N-methylamidomethyl)-2-(3',4'-dimethoxyphenyl)cyclohexyl acetate
CAS No.:121537-77-7
Molecular Formula:C₂₁H₂₉NO₇
Molecular Weight:407.464
Hs Code.:

Synonyms:(1RS,2SR)-5,5-ethylenedioxy-2-(N-methylamidomethyl)-2-(3',4'-dimethoxyphenyl)cyclohexyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1RS,2SR)-5,5-ethylenedioxy-2-(N-methylamidomethyl)-2-(3',4'-dimethoxyphenyl)cyclohexyl acetate

Chemical Property:

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Technology Process of (1RS,2SR)-5,5-ethylenedioxy-2-(N-methylamidomethyl)-2-(3',4'-dimethoxyphenyl)cyclohexyl acetate

There total 3 articles about (1RS,2SR)-5,5-ethylenedioxy-2-(N-methylamidomethyl)-2-(3',4'-dimethoxyphenyl)cyclohexyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70779-53-2,114047-06-2
Acetic acid (7R,8S)-8-allyl-8-(3,4-dimethoxy-phenyl)-1,4-dioxa-spiro[4.5]dec-7-yl ester

: 121537-77-7
(1RS,2SR)-5,5-ethylenedioxy-2-(N-methylamidomethyl)-2-(3',4'-dimethoxyphenyl)cyclohexyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 80.8 percent / NaIO₄, RuCl₃(H₂O)n / CCl₄; H₂O / 2 h / Ambient temperature

2: 71.4 percent / 1percent aq. KMnO₄ / acetone / 1 h / Ambient temperature

3: 1.) ClCOOC₂H₅, Et₃N / 1.) CHCl₃, room temp. 45 min; 2.) CHCl₃, room temp. 1 h

With ruthenium trichloride; potassium permanganate; sodium periodate; chloroformic acid ethyl ester; triethylamine; In tetrachloromethane; water; acetone;

Reference yield:

: 70779-54-3,81254-93-5
Acetic acid (7R,8S)-8-(3,4-dimethoxy-phenyl)-8-(2-oxo-ethyl)-1,4-dioxa-spiro[4.5]dec-7-yl ester

: 121537-77-7
(1RS,2SR)-5,5-ethylenedioxy-2-(N-methylamidomethyl)-2-(3',4'-dimethoxyphenyl)cyclohexyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 71.4 percent / 1percent aq. KMnO₄ / acetone / 1 h / Ambient temperature

2: 1.) ClCOOC₂H₅, Et₃N / 1.) CHCl₃, room temp. 45 min; 2.) CHCl₃, room temp. 1 h

With potassium permanganate; chloroformic acid ethyl ester; triethylamine; In acetone;

Reference yield:

: 121537-76-6
2-carboxymethyl-5,5-ethylenedioxy-2-(3',4'-dimethoxyphenyl)cyclohexyl acetate

: 74-89-5
methylamine

: 121537-77-7
(1RS,2SR)-5,5-ethylenedioxy-2-(N-methylamidomethyl)-2-(3',4'-dimethoxyphenyl)cyclohexyl acetate

Guidance literature:: With chloroformic acid ethyl ester; triethylamine; Yield given. Multistep reaction; 1.) CHCl₃, room temp. 45 min; 2.) CHCl₃, room temp. 1 h;