(2-formyl-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

Base Information

Chemical Name:(2-formyl-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone
CAS No.:1258391-60-4
Molecular Formula:C₂₄H₂₆Cl₂O₆
Molecular Weight:481.373
Hs Code.:

Synonyms:(2-formyl-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

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Chemical Property of (2-formyl-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

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Technology Process of (2-formyl-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

There total 1 articles about (2-formyl-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1258391-57-9
(2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

: 109-94-4
formic acid ethyl ester

: 1258391-60-4
(2-formyl-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

Guidance literature:: (2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone; With n-butyllithium; magnesium bromide ethyl etherate; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

formic acid ethyl ester; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1002/anie.201003755

Reference yield: 84.0%

: 1258391-60-4
(2-formyl-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

: 1258391-66-0
3-(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-5,7-dimethoxy-1H-indene-4-carbaldehyde

Guidance literature:: With boron dimethyl-trifluoro sulphide; In dichloromethane; at 0 ℃; for 0.75h; Inert atmosphere;
DOI:10.1002/anie.201003755

Reference yield: 50.0%

: 1258391-60-4
(2-formyl-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

: 1258391-64-8
(2-formyl-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2-hydroxy-6-methoxy-4-methylphenyl)methanone

Guidance literature:: With boron dimethyl-trifluoro sulphide; dimethylsulfide; In dichloromethane; at -30 ℃; for 1.25h; Inert atmosphere;
DOI:10.1002/anie.201003755