2-(3-benzylsulfanyl-2-methoxy-phenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Base Information

Chemical Name:2-(3-benzylsulfanyl-2-methoxy-phenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane
CAS No.:1184298-16-5
Molecular Formula:C₂₀H₂₅BO₃S
Molecular Weight:356.294
Hs Code.:

Synonyms:2-(3-benzylsulfanyl-2-methoxy-phenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Suppliers and Price of 2-(3-benzylsulfanyl-2-methoxy-phenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-(3-benzylsulfanyl-2-methoxy-phenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of 2-(3-benzylsulfanyl-2-methoxy-phenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

There total 1 articles about 2-(3-benzylsulfanyl-2-methoxy-phenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1184298-15-4
1-benzylsulfanyl-3-bromo-2-methoxy-benzene

: 73183-34-3
bis(pinacol)diborane

: 1184298-16-5
2-(3-benzylsulfanyl-2-methoxy-phenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Guidance literature:: With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In dimethyl sulfoxide; at 110 ℃; for 16h; Inert atmosphere;

Reference yield: 29.0%

: 81971-38-2
3-bromo-1-methyl-1H-pyridin-2-one

: 1184298-16-5
2-(3-benzylsulfanyl-2-methoxy-phenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 1184298-17-6
3-(3-benzylsulfanyl-2-methoxy-phenyl)-1-methyl-1H-pyridin-2-one

Guidance literature:: With barium hydroxide octahydrate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In water; dimethyl sulfoxide; at 110 ℃; for 4h; Inert atmosphere;

Reference yield:

: 81971-38-2
3-bromo-1-methyl-1H-pyridin-2-one

: 1184298-16-5
2-(3-benzylsulfanyl-2-methoxy-phenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 1184298-18-7
2-methoxy-3-(1-methyl-2-oxo-1 ,2-dihydro-pyridin-3-yl)-benzenesulfonyl chloride

: 1184298-19-8
3-(5-chloro-1-methyl-2-oxo-1 ,2-dihydro-pyridin-3-yl)-2-methoxy-benzenesulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: barium hydroxide octahydrate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; dimethyl sulfoxide / 4 h / 110 °C / Inert atmosphere

2: sulfuryl dichloride; water; acetic acid / dichloromethane / 0.42 h / 0 - 20 °C

With sulfuryl dichloride; barium hydroxide octahydrate; water; acetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In dichloromethane; water; dimethyl sulfoxide;