ethyl N-<2--4-methoxyphenyl>acetamidate

Base Information

Chemical Name:ethyl N-<2--4-methoxyphenyl>acetamidate
CAS No.:86439-30-7
Molecular Formula:C₂₀H₂₆N₂O₅S
Molecular Weight:406.503
Hs Code.:

ethyl N-<2-<N-(2-hydroxyethyl)-N-tosylamino>-4-methoxyphenyl>acetamidate

Synonyms:ethyl N-<2--4-methoxyphenyl>acetamidate

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Chemical Property of ethyl N-<2--4-methoxyphenyl>acetamidate

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Technology Process of ethyl N-<2--4-methoxyphenyl>acetamidate

There total 3 articles about ethyl N-<2--4-methoxyphenyl>acetamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 78-39-7
Triethyl orthoacetate

: 86439-28-3
2'-amino-N-(2-hydroxyethyl)-4'-methoxytosylanilide

: 86439-30-7
ethyl N-<2--4-methoxyphenyl>acetamidate

Guidance literature:: for 6h; Heating;
DOI:10.1016/S0040-4020(01)88550-1

Reference yield:

: 3360-81-4
N-(4-methoxy-2-nitrophenyl)-4-methylbenzenesulfonamide

: 86439-30-7
ethyl N-<2--4-methoxyphenyl>acetamidate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Na / 1.) methanol, reflux, 0.5 h; 2.) DMF, 120 deg C, 10 h

2: 92 percent / 8percent Pd/C / propan-2-ol / 760 Torr / Ambient temperature

3: 49 percent / 6 h / Heating

With sodium; palladium on activated charcoal; In isopropyl alcohol;
DOI:10.1016/S0040-4020(01)88550-1

Reference yield:

: 86439-27-2
N-(2-hydroxyethyl)-4'-methoxy-2'-nitrotosylanilide

: 86439-30-7
ethyl N-<2--4-methoxyphenyl>acetamidate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 8percent Pd/C / propan-2-ol / 760 Torr / Ambient temperature

2: 49 percent / 6 h / Heating

palladium on activated charcoal; In isopropyl alcohol;
DOI:10.1016/S0040-4020(01)88550-1