Technology Process of C35H50N4S
There total 6 articles about C35H50N4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Lawessons reagent;
In
toluene;
for 12h;
Inert atmosphere;
Reflux;
DOI:10.1002/ejoc.201200303
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium hydrogencarbonate; N-ethyl-N,N-diisopropylamine / 1,4-dioxane; water / 3 h / 0 - 20 °C
2: chloroformic acid ethyl ester; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C
3: dichloromethane / 20 °C
4: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 20 °C / 760.05 Torr
5: ytterbium(III) triflate / toluene / 3 h / 120 °C / Microwave irradiation
6: Lawessons reagent / toluene / 12 h / Inert atmosphere; Reflux
With
Lawessons reagent; palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; potassium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; ytterbium(III) triflate;
In
1,4-dioxane; methanol; dichloromethane; water; toluene;
DOI:10.1002/ejoc.201200303
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 20 °C / 760.05 Torr
2: ytterbium(III) triflate / toluene / 3 h / 120 °C / Microwave irradiation
3: Lawessons reagent / toluene / 12 h / Inert atmosphere; Reflux
With
Lawessons reagent; palladium 10% on activated carbon; hydrogen; ytterbium(III) triflate;
In
methanol; toluene;
DOI:10.1002/ejoc.201200303
