2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-p-tolylacetamide

Base Information

Chemical Name:2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-p-tolylacetamide
CAS No.:1263104-19-3
Molecular Formula:C₂₃H₂₀N₆O
Molecular Weight:396.451
Hs Code.:

Synonyms:2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-p-tolylacetamide

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Chemical Property of 2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-p-tolylacetamide

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Technology Process of 2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-p-tolylacetamide

There total 3 articles about 2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-p-tolylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.29%

: 5343-65-7
2-bromo-N-p-tolylacetamide

: 1263104-14-8
8-methyl-6-phenyl-1,6-dihydrodipyrazolo[3,4-b:3',4'-d]pyridine

: 1263104-19-3
2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-p-tolylacetamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 55 - 60 ℃; for 6h;
DOI:10.1007/s10895-010-0622-4

Reference yield:

: 1263104-04-6
(4-chloro-3-methyl-1-phenyl-1H-pyrazolo[3,4-b]pyridin-5-yl)methanone

: 1263104-19-3
2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-p-tolylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / ethanol / 8 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 6 h / 55 - 60 °C

With potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1007/s10895-010-0622-4

Reference yield:

: 81153-44-8
4-chloro-3-methyl-1-phenyl-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid ethyl ester

: 1263104-19-3
2-(8-methyl-6-phenyldipyrazolo[3,4-b:3',4'-d]pyridin-1(6H)-yl)-N-p-tolylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -78 °C

2: potassium carbonate / ethanol / 8 h / Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 6 h / 55 - 60 °C

With diisobutylaluminium hydride; potassium carbonate; In ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1007/s10895-010-0622-4