(R)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

Base Information

Chemical Name:(R)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester
CAS No.:126662-25-7
Molecular Formula:C₁₆H₃₂NO₃PS₂
Molecular Weight:381.541
Hs Code.:

Synonyms:(R)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

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Chemical Property of (R)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

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Technology Process of (R)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

There total 5 articles about (R)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 110-91-8,99108-56-2
morpholine

: 126662-26-8
(R)_P-Ethoxy-L-menthoxythioxaphosphoranesulphenyl chloride

: 126662-25-7
(R)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

Guidance literature:: In hexane; at 0 - 5 ℃;
DOI:10.1016/S0040-4020(98)00529-8

Reference yield:

: Phosphorochloridous acid ethyl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: 126662-25-7
(R)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂S / hexane / 5 h / 0 - 5 °C

2: 1.5 g / Et₃N / hexane

With hydrogen sulfide; triethylamine; In hexane;
DOI:10.1016/S0040-4020(98)00529-8