Ir(III)(1-phenylisoquinoline^(1-))2(picolinate)

Base Information

Chemical Name:Ir(III)(1-phenylisoquinoline^(1-))2(picolinate)
CAS No.:1186193-36-1
Molecular Formula:C₃₆H₂₄IrN₃O₂
Molecular Weight:722.825
Hs Code.:

Ir(III)(1-phenylisoquinoline<sup>(1-)</sup>)2(picolinate)

Synonyms:Ir(III)(1-phenylisoquinoline^(1-))2(picolinate)

Suppliers and Price of Ir(III)(1-phenylisoquinoline^(1-))2(picolinate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Ir(III)(1-phenylisoquinoline^(1-))2(picolinate)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Ir(III)(1-phenylisoquinoline^(1-))2(picolinate)

There total 1 articles about Ir(III)(1-phenylisoquinoline^(1-))2(picolinate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 98-98-6
2-Picolinic acid

: 3297-72-1
1-phenylisoquinoline

: iridium(III) chloride hydrate

: 1186193-36-1
Ir(III)(1-phenylisoquinoline^(1-))2(picolinate)

Guidance literature:: With sodium carbonate; In 2-ethoxy-ethanol; Ir salt mixed with isoquinoline derivative in 2-ethoxyethanol-H2O; refluxed for 6-7 h; cooled to room temp.; H2O added; filtered; ppt. washed (hexane, Et2O); mixed with picolinic acid, Na2CO3 and 2-ethoxyethanol under inert atmosphere; refluxed (4-5 h); cooled to room temp.; solvent evapd. under high vac.; dissolved in CH2Cl2; org. phase washed with H2O; dried (Na2SO4); solvent evapd.; purified by column chromy. (silica gel, CH2Cl2-MeOH);
DOI:10.1039/c1nj20446g