hydrido[bis(pentafluorophenyl)][2-(2,2,6,6-tetramethylpiperidinium-1-yl)phenyl]borate^(1-)

Base Information

• Chemical Name: hydrido[bis(pentafluorophenyl)][2-(2,2,6,6-tetramethylpiperidinium-1-yl)phenyl]borate^(1-)
• CAS No.: 1391933-27-9
• Molecular Formula: C₂₇H₂₃BF₁₀N*H
• Molecular Weight: 563.289

Synonyms:hydrido[bis(pentafluorophenyl)][2-(2,2,6,6-tetramethylpiperidinium-1-yl)phenyl]borate^(1-)

Chemical Property of hydrido[bis(pentafluorophenyl)][2-(2,2,6,6-tetramethylpiperidinium-1-yl)phenyl]borate^(1-)

Chemical Property:

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Technology Process of hydrido[bis(pentafluorophenyl)][2-(2,2,6,6-tetramethylpiperidinium-1-yl)phenyl]borate^(1-)

There total 4 articles about hydrido[bis(pentafluorophenyl)][2-(2,2,6,6-tetramethylpiperidinium-1-yl)phenyl]borate^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-{2-[bis(pentafluorophenyl)boryl]phenyl}-2,2,6,6-tetramethylpiperidine (1391927-76-6) → hydrido[bis(pentafluorophenyl)][2-(2,2,6,6-tetramethylpiperidinium-1-yl)phenyl]borate(1-) (1391933-27-9)

Guidance literature:

With hydrogen; In toluene; at 20 ℃; for 0.5h; under 1500.15 Torr; Inert atmosphere;

DOI:10.1039/c2dt30926b

Reference yield: 100.0%

1-{2-[bis(pentafluorophenyl)boryl]phenyl}-2,2,6,6-tetramethylpiperidine (1391927-76-6) + hydrogen (1333-74-0) → hydrido[bis(pentafluorophenyl)][2-(2,2,6,6-tetramethylpiperidinium-1-yl)phenyl]borate(1-) (1391933-27-9)

Guidance literature:

In benzene-d6; C6D6, H2, room temp.;

DOI:10.1039/c2dt30926b

Reference yield:

2,2,6,6-tetramethyl-piperidine (768-66-1) → hydrido[bis(pentafluorophenyl)][2-(2,2,6,6-tetramethylpiperidinium-1-yl)phenyl]borate(1-) (1391933-27-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / -40 - -20 °C / Inert atmosphere

1.2: -50 - -40 °C / Inert atmosphere

2.1: n-butyllithium / hexane / 4 h / 5 °C / Inert atmosphere

3.1: toluene / -80 - 20 °C / Inert atmosphere

4.1: hydrogen / toluene / 0.5 h / 20 °C / 1500.15 Torr / Inert atmosphere

With n-butyllithium; hydrogen; In tetrahydrofuran; hexane; toluene;

DOI:10.1039/c2dt30926b

upstream raw materials:

2,2,6,6-tetramethyl-piperidine

[2-(2,2,6,6-tetramethylpiperidin-1-yl)phenyl]lithium

bis(pentafluorophenyl)boron chloride

1-{2-[bis(pentafluorophenyl)boryl]phenyl}-2,2,6,6-tetramethylpiperidine

Downstream raw materials:

1-{2-[bis(pentafluorophenyl)boryl]phenyl}-2,2,6,6-tetramethylpiperidine

Pentafluorobenzene

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