(1R,2S,5R)-(-)-(Z)-cinnamyl menthyl selenide

Base Information

Chemical Name:(1R,2S,5R)-(-)-(Z)-cinnamyl menthyl selenide
CAS No.:1462351-69-4
Molecular Formula:C₁₉H₂₈Se
Molecular Weight:335.391
Hs Code.:

Synonyms:(1R,2S,5R)-(-)-(Z)-cinnamyl menthyl selenide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,5R)-(-)-(Z)-cinnamyl menthyl selenide

Chemical Property:

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Technology Process of (1R,2S,5R)-(-)-(Z)-cinnamyl menthyl selenide

There total 4 articles about (1R,2S,5R)-(-)-(Z)-cinnamyl menthyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 21087-29-6
trans-3-phenylprop-2-enyl chloride

: (1R,2S,5R)-(-)-menthyl selenol

: 1462351-69-4
(1R,2S,5R)-(-)-(Z)-cinnamyl menthyl selenide

Guidance literature:: (1R,2S,5R)-(-)-menthyl selenol; With n-butyllithium; In tetrahydrofuran; at -25 ℃; for 0.5h; Inert atmosphere;

trans-3-phenylprop-2-enyl chloride; In tetrahydrofuran; at 0 - 50 ℃; for 1h;
DOI:10.1016/j.tetasy.2013.07.018

Reference yield:

: 2216-51-5
(-)-menthol

: 1462351-69-4
(1R,2S,5R)-(-)-(Z)-cinnamyl menthyl selenide

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrachloromethane; triphenylphosphine / 16 h / Reflux

2.1: sodium hydroxide; selenium; hydrazine hydrate

3.1: n-butyllithium / tetrahydrofuran / 0.5 h / -25 °C / Inert atmosphere

3.2: 1 h / 0 - 50 °C

With tetrachloromethane; selenium; n-butyllithium; hydrazine hydrate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2013.07.018

Reference yield:

: 13371-12-5
neomenthyl chloride

: 1462351-69-4
(1R,2S,5R)-(-)-(Z)-cinnamyl menthyl selenide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide; selenium; hydrazine hydrate

2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -25 °C / Inert atmosphere

2.2: 1 h / 0 - 50 °C

With selenium; n-butyllithium; hydrazine hydrate; sodium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2013.07.018